2-((4-CHLOROPHENYL)SULFONYL)-3,3-DIMETHYLTHIOPROP-2-ENENITRILE

Base Information

• Chemical Name: 2-((4-CHLOROPHENYL)SULFONYL)-3,3-DIMETHYLTHIOPROP-2-ENENITRILE
• CAS No.: 124392-37-6
• Molecular Formula: C11H10ClNO2S3
• Molecular Weight: 319.857
• Mol file: 124392-37-6.mol

Synonyms:2-(4-Chloro-benzenesulfonyl)-3,3-bis-methylsulfanyl-acrylonitrile;1-(4-chlorophenyl)sulfonyl-1-cyano-2,2-bis(methylthio)ethylene;

Chemical Property of 2-((4-CHLOROPHENYL)SULFONYL)-3,3-DIMETHYLTHIOPROP-2-ENENITRILE

Chemical Property:

• PSA: 116.91000
• LogP: 4.61318

Purity/Quality:

2-((4-chlorophenyl)sulfonyl)-3,3-dimethylthioprop-2-enenitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-((4-CHLOROPHENYL)SULFONYL)-3,3-DIMETHYLTHIOPROP-2-ENENITRILE

There total 2 articles about 2-((4-CHLOROPHENYL)SULFONYL)-3,3-DIMETHYLTHIOPROP-2-ENENITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

carbon disulfide (75-15-0,12122-00-8) + 2-(4-chlorobenzenesulfonyl)acetonitrile (1851-09-8) + methyl iodide (74-88-4) → 2-(4-chlorobenzenesulfonyl)-3,3-bis-methylsulfanyl-acrylonitrile (124392-37-6)

Guidance literature:

carbon disulfide; 2-(4-chlorobenzenesulfonyl)acetonitrile; With sodium hydride; In dimethyl sulfoxide; at 0 - 20 ℃; for 1h;

methyl iodide; In dimethyl sulfoxide; at 0 - 20 ℃; for 18h;

Reference yield:

→ 2-(4-chlorobenzenesulfonyl)-3,3-bis-methylsulfanyl-acrylonitrile (124392-37-6)

Guidance literature:

Reference yield: 65.0%

2-(4-chlorobenzenesulfonyl)-3,3-bis-methylsulfanyl-acrylonitrile (124392-37-6) + 4-Ethoxyaniline (156-43-4) → (E)-2-(4-Chloro-benzenesulfonyl)-3-(4-ethoxy-phenylamino)-3-methylsulfanyl-acrylonitrile (124392-32-1)

Guidance literature:

In ethanol; 1) 1 h, reflux, 2) 24 h, room temperature;

upstream raw materials:

carbon disulfide

2-(4-chlorobenzenesulfonyl)acetonitrile

methyl iodide

Downstream raw materials:

(E)-2-(4-Chloro-benzenesulfonyl)-3-(2-methoxy-phenylamino)-3-methylsulfanyl-acrylonitrile

(E)-2-(4-Chloro-benzenesulfonyl)-3-(4-methoxy-phenylamino)-3-methylsulfanyl-acrylonitrile

(E)-2-(4-Chloro-benzenesulfonyl)-3-methylsulfanyl-3-phenylamino-acrylonitrile

(E)-2-(4-Chloro-benzenesulfonyl)-3-(4-ethoxy-phenylamino)-3-methylsulfanyl-acrylonitrile

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