C₅₉H₅₆O₈

Base Information

Chemical Name:C₅₉H₅₆O₈
CAS No.:197805-80-4
Molecular Formula:C₅₉H₅₆O₈
Molecular Weight:893.089
Hs Code.:

C<sub>59</sub>H<sub>56</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₅₉H₅₆O₈

Chemical Property:

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Technology Process of C₅₉H₅₆O₈

There total 7 articles about C₅₉H₅₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2467-03-0
2-[(4-hydroxyphenyl)methyl]phenol

: 197805-80-4
C₅₉H₅₆O₈

Guidance literature:: Multi-step reaction with 7 steps

1: 65 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

2: 98 percent / imidazole / dimethylformamide / 24 h

3: 86 percent / BF₃*OEt₂ / CHCl₃ / 17 h / 0 °C

4: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 min, 2.) C₆H₆, reflux, 20.5 h

5: 58 percent / K₂CO₃ / acetone / 23.5 h / Heating

6: 95 percent / TBAF / tetrahydrofuran / 4 h

7: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 in, 2.) C₆H₆, reflux, 20 h

With 1H-imidazole; boron trifluoride diethyl etherate; ethylmagnesium bromide; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(97)00903-4

Reference yield:

: 197805-63-3
2-[4-(tert-Butyl-dimethyl-silanyloxy)-benzyl]-phenol

: 197805-80-4
C₅₉H₅₆O₈

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / imidazole / dimethylformamide / 24 h

2: 86 percent / BF₃*OEt₂ / CHCl₃ / 17 h / 0 °C

3: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 min, 2.) C₆H₆, reflux, 20.5 h

4: 58 percent / K₂CO₃ / acetone / 23.5 h / Heating

5: 95 percent / TBAF / tetrahydrofuran / 4 h

6: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 in, 2.) C₆H₆, reflux, 20 h

With 1H-imidazole; boron trifluoride diethyl etherate; ethylmagnesium bromide; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(97)00903-4

Reference yield:

: 197805-68-8
4-[2-(tert-Butyl-diphenyl-silanyloxy)-benzyl]-phenol

: 197805-80-4
C₅₉H₅₆O₈

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 min, 2.) C₆H₆, reflux, 20.5 h

2: 58 percent / K₂CO₃ / acetone / 23.5 h / Heating

3: 95 percent / TBAF / tetrahydrofuran / 4 h

4: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 in, 2.) C₆H₆, reflux, 20 h

With ethylmagnesium bromide; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(97)00903-4