1-ferrocenyl-1-methoxy-1-phenylpropyne

Base Information

Chemical Name:1-ferrocenyl-1-methoxy-1-phenylpropyne
CAS No.:672958-80-4
Molecular Formula:C₂₀H₁₈FeO
Molecular Weight:330.209
Hs Code.:

Synonyms:1-ferrocenyl-1-methoxy-1-phenylpropyne

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Chemical Property of 1-ferrocenyl-1-methoxy-1-phenylpropyne

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Technology Process of 1-ferrocenyl-1-methoxy-1-phenylpropyne

There total 1 articles about 1-ferrocenyl-1-methoxy-1-phenylpropyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.2%

: 672958-79-1
1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne

: 672958-80-4
1-ferrocenyl-1-methoxy-1-phenylpropyne

Guidance literature:: With potassium hydroxide; In methanol; a suspn. of silylated ether and solid KOH in MeOH was stirred under Ar at room temp. for 12 h; evapd. in vacuo, residue was dissolved in ether, soln. washed with aq. NaHCO3 and water, dried over Na2SO4 and evapd.; elem. anal.;

Reference yield: 72.7%

: 1272-44-2
benzoylferrocene

: 672958-80-4
1-ferrocenyl-1-methoxy-1-phenylpropyne

: 672958-81-5
1,4-diferrocenyl-4-methoxy-1,4-diphenylbut-2-ynol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; n-BuLi soln. was added at -60°C under Ar to a THF soln. of the propyne, the stirred was allowed to warm to room temp., FcCOPh was added under Ar, the mixt. was stirred for 18 h; water was added, solvents were removed in vacuo, the residue was dissolved in ether, soln. washed with water, dried over Na2SO4, evapd., residuewas chromd. on basic alumina (eluent 2:1 hexane-ether); elem. anal.;

Reference yield: 55.7%

: 672958-80-4
1-ferrocenyl-1-methoxy-1-phenylpropyne

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 672959-02-3
3-ferrocenyl-1-iodo-3-methoxy-3-phenylpropyne

Guidance literature:: With n-butyllithium; In tetrahydrofuran; pentane; n-BuLi in pentane was added at -60°C under Ar to a THF soln. of Fc(Ph)(OMe)CCCH, the mixt. was warmed to room temp., I2 was added under Ar, the mixt. was stirred for 18 h; water was added, volatiles removed in vacuo, residue was dissolved in ether, soln. washed with aq. NaHCO3 and water, dried over Na2SO4, evapd., residue was chromd. on basic alumina (eluent 2:1 hexane-ether); elem. anal.;