Sn(C₆Cl₅)4

Base Information

Chemical Name:Sn(C₆Cl₅)4
CAS No.:15527-40-9
Molecular Formula:C₂₄Cl₂₀Sn
Molecular Weight:1116.03
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Sn(C₆Cl₅)4

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Technology Process of Sn(C₆Cl₅)4

There total 2 articles about Sn(C₆Cl₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 7646-78-8
tin(IV) chloride

: 6782-80-5
pentachlorophenyllithium

: 15527-40-9
Sn(C₆Cl₅)4

Guidance literature:: In diethyl ether; byproducts: LiCl; (Ar, Schlenk technique); addn. of ethereal soln. of lithium compd. to ethereal soln. of tin compd. at -60°C, stirring at -60°C for1 h and at room temp. for 8 h; evapn., addn. of toluene, filtration, concg., isolation of crystals, elem. anal.;
DOI:10.1016/j.jorganchem.2010.07.019

Reference yield:

: 31279-13-7
pentachlorophenylmagnesium chloride

: 7646-78-8
tin(IV) chloride

: 15527-40-9
Sn(C₆Cl₅)4

Guidance literature:: In tetrahydrofuran; hexane; xylene; 8 fold amount of C6Cl5MgCl, mixing at room temp. for 3 h, then boiling under reflux for 2 h, then replacement of hexane with xylol and boiling under reflux for 2 h;
DOI:10.1016/S0022-328X(00)91074-X