5-Bromo-3-methylpentyl acetate

Base Information

Chemical Name:5-Bromo-3-methylpentyl acetate
CAS No.:125161-79-7
Molecular Formula:C8H15BrO2
Molecular Weight:223.11
Hs Code.:
Mol file:125161-79-7.mol

Synonyms:5-Bromo-3-methylpentyl acetate;1-acetoxy-5-bromo-3-methylpentane;3-methyl-5-bromo-1-acetoxypentane;Acetic acid,5-bromo-3-methylpenthyl ester;

Suppliers and Price of 5-Bromo-3-methylpentyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5-Bromo-3-methylpentyl acetate

Chemical Property:

PSA：26.30000
LogP:2.36070

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Bromo-3-methylpentyl acetate

There total 1 articles about 5-Bromo-3-methylpentyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4717-96-8
4-methyltetrahydropyran

: 506-96-7
Acetyl bromide

: 125161-79-7
1-acetoxy-5-bromo-3-methylpentane

Guidance literature:: With zinc(II) chloride; at 120 ℃; for 2h;
DOI:10.1007/BF00598420 DOI:10.1007/BF00956974

Reference yield:

: 125161-79-7
1-acetoxy-5-bromo-3-methylpentane

: 3613-30-7
7-methoxy-3,7-dimethyloctanal

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / benzene; dimethylformamide / 3 h / 20 °C

1.2: 96 percent / benzene; dimethylformamide / 12 h / Heating

2.1: 81 percent / LiI / dimethylformamide / 12 h / Heating

3.1: n-BuLi / tetrahydrofuran; hexane / 1 h / 20 °C

3.2: 85 percent / tetrahydrofuran; hexane / 0 - 20 °C

4.1: Hg(OAc)2 / 25 h / 5 - 20 °C

4.2: 97 percent / NaOH; NaBH₄ / H₂O / 3 h / 0 - 20 °C

5.1: 90 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h / 20 °C

With n-butyllithium; mercury(II) diacetate; sodium hydride; pyridinium chlorochromate; lithium iodide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1023/A:1014439914429

Reference yield:

: 125161-79-7
1-acetoxy-5-bromo-3-methylpentane

: 60018-13-5,81738-03-6,124440-53-5,25795-46-4,5988-91-0
3,7-dimethyl-1-octanal

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaH / benzene; dimethylformamide / 3 h / 20 °C

1.2: 96 percent / benzene; dimethylformamide / 12 h / Heating

2.1: 81 percent / LiI / dimethylformamide / 12 h / Heating

3.1: n-BuLi / tetrahydrofuran; hexane / 1 h / 20 °C

3.2: 85 percent / tetrahydrofuran; hexane / 0 - 20 °C

4.1: 90 percent / KOH / methanol / 4 h / Heating

5.1: H₂ / Pd/C / methanol / 5 h

6.1: 1.69 g / pyridinium chlorochromate / CH₂Cl₂ / 2 h / 20 °C

With potassium hydroxide; n-butyllithium; hydrogen; sodium hydride; pyridinium chlorochromate; lithium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1023/A:1014439914429