dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II)

Base Information

Chemical Name:dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II)
CAS No.:346608-28-4
Molecular Formula:C₁₁H₁₂Cl₂N₄Pt
Molecular Weight:466.229
Hs Code.:

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Chemical Property of dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II)

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Technology Process of dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II)

There total 1 articles about dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 198347-67-0
1-methyl-2-(4'-methylphenylazo)imidazole

: 346608-28-4
dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II)

Guidance literature:: In water; acetonitrile; to MeCN-H2O (1:1) soln. K2PtCl4 1-methyl-2-((arylazo)imidazole) in the same solvent was added dropwise and refluxed for 30 h; solvent was evapd. slowly, ppt. was filtered, washed with cold MeCN-H2O (1:1), dried, dissolved in CH2Cl2 and chromed. on silica (C6H6-MeCN 2:1); elem. anal.;

Reference yield: 41.0%

: 346608-28-4
dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II)

: 7732-18-5
water

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: catecholato(1-methyl-2-(p-tolylazo)imidazole)platinum(II)*0.5H₂O

Guidance literature:: With triethylamine; In methanol; chloroform; Pt(MeaaiMe)Cl2 was dissolved in CHCl3-MeOH (1:1), soln. was degassed by bubbling N2, pyrocatechol in MeOH was added slowly followed by NEt3 under N2, soln. was stirred for 1 h and N2 was bubbled slowly for another 1 h; ppt. was filtered, washed with cold MeOH, dried in vacuo, dissolved in CH2Cl2 and chromed. on silica (C6H6-MeCN 3:2); elem. anal.;

Reference yield:

: 346608-28-4
dichloro(1-methyl-2-(p-tolylazo)imidazole)platinum(II)

: 1198-55-6
o-chloranil

: 7732-18-5
water

: [Pt(MeaaiMe)(tccat)]*0.5H₂O

Guidance literature:: With triethylamine; In methanol; chloroform; Pt(MeaaiMe)Cl2 was dissolved in CHCl3-MeOH (1:1), soln. was degassed by bubbling N2, catechol in MeOH was added slowly followed by NEt3 under N2, soln. was stirred for 1 h and N2 was bubbled slowly for another 1 h; ppt. was filtered, washed with cold MeOH, dried in vacuo, dissolved in CH2Cl2 and chromed. on silica (C6H6-MeCN 3:2); elem. anal.;