Benzoic acid, 3-amino-5-(methoxymethoxy)-4-methyl-, methyl ester

Base Information

Chemical Name:Benzoic acid, 3-amino-5-(methoxymethoxy)-4-methyl-, methyl ester
CAS No.:125229-15-4
Molecular Formula:C11H15NO4
Molecular Weight:225.244
Hs Code.:
DSSTox Substance ID:DTXSID30448097
Nikkaji Number:J291.495F
Mol file:125229-15-4.mol

Synonyms:125229-15-4;Benzoic acid, 3-amino-5-(methoxymethoxy)-4-methyl-, methyl ester;DTXSID30448097;3-Methoxymethoxy-4-methyl-5-aminobenzoic acid methyl ester

Suppliers and Price of Benzoic acid, 3-amino-5-(methoxymethoxy)-4-methyl-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzoic acid, 3-amino-5-(methoxymethoxy)-4-methyl-, methyl ester

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:225.10010796
Heavy Atom Count:16
Complexity:234

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1OCOC)C(=O)OC)N

Technology Process of Benzoic acid, 3-amino-5-(methoxymethoxy)-4-methyl-, methyl ester

There total 3 articles about Benzoic acid, 3-amino-5-(methoxymethoxy)-4-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 125229-14-3
methyl 3-methoxymethyloxy-4-methyl-5-nitrobenzene

: 125229-15-4
methyl 3-amino-5-methoxymethoxy-4-methylbenzoate

Guidance literature:: With hydrogen; 10percent Pd/C; In methanol; at 20 ℃; for 2h; under 3102.97 Torr;
DOI:10.1021/jo0206521

Reference yield:

: 54591-64-9
3-hydroxy-4-methyl-5-nitrobenzoic acid

: 125229-15-4
methyl 3-amino-5-methoxymethoxy-4-methylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / sulfuric acid / H₂O / 20 h / Heating

2: 98 percent / P₂O₅ / CH₂Cl₂ / 20 °C

3: 95 percent / H₂ / 10percent Pd/C / methanol / 2 h / 20 °C / 3102.97 Torr

With sulfuric acid; hydrogen; phosphorus pentoxide; 10percent Pd/C; In methanol; dichloromethane; water;
DOI:10.1021/jo0206521

Reference yield:

: 125229-13-2
3-hydroxy-4-methyl-5-nitrobenzoic acid methyl ester

: 125229-15-4
methyl 3-amino-5-methoxymethoxy-4-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / P₂O₅ / CH₂Cl₂ / 20 °C

2: 95 percent / H₂ / 10percent Pd/C / methanol / 2 h / 20 °C / 3102.97 Torr

With hydrogen; phosphorus pentoxide; 10percent Pd/C; In methanol; dichloromethane;
DOI:10.1021/jo0206521