(E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine

Base Information

• Chemical Name: (E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine
• CAS No.: 175025-75-9
• Molecular Formula: C₁₅H₂₀N₂O
• Molecular Weight: 244.337

Synonyms:

Chemical Property of (E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine

Chemical Property:

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Technology Process of (E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine

There total 1 articles about (E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-{2-[(E)-2-oxo-2-phenylethylidene]-1-pyrrolidinyl}propanenitrile (175025-74-8) → (E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine (175025-75-9)

Guidance literature:

With sodium hydroxide; nickel-aluminium alloy; In ethanol; for 0.833333h; Product distribution; Ambient temperature; var. reagents; other vinylogous amides; chemoselectivity;

DOI:10.1016/0040-4020(95)01051-3

Reference yield: 59.0%

benzoyl chloride (98-88-4) + (E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine (175025-75-9) → (E)-1-(3-benzoylaminopropyl)-2-benzoylmethylenepyrrolidine

Guidance literature:

With pyridine; for 1.83333h;

DOI:10.1016/0040-4020(95)01051-3

Reference yield: 49.0%

Hexanoyl chloride (142-61-0) + (E)-1-(3-aminopropyl)-2-benzoylmethylenepyrrolidine (175025-75-9) → (E)-2-benzoylmethylene-1-(3-hexanoylaminopropyl)pyrrolidine

Guidance literature:

With pyridine; for 1.5h;

DOI:10.1016/0040-4020(95)01051-3

upstream raw materials:

3-{2-[(E)-2-oxo-2-phenylethylidene]-1-pyrrolidinyl}propanenitrile

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