C₃H₃N₂CH₂NC₃H₃NC(CH₃)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=(C₃H₃N₂CH₂NC₃H₃NC(CH₃)3)B(C₆H₅)4

Base Information

Chemical Name:C₃H₃N₂CH₂NC₃H₃NC(CH₃)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=(C₃H₃N₂CH₂NC₃H₃NC(CH₃)3)B(C₆H₅)4
CAS No.:1191987-61-7
Molecular Formula:C₁₁H₁₇N₄*C₂₄H₂₀B
Molecular Weight:524.517
Hs Code.:

C<sub>3</sub>H<sub>3</sub>N<sub>2</sub>CH<sub>2</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)3<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=(C<sub>3</sub>H<sub>3</sub>N<sub>2</sub>CH<sub>2</sub>NC<sub>3</sub>H<sub>3</sub>NC(CH<sub>3</sub>)3)B(C<sub>6</sub>H<sub>5</sub>)4

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Chemical Property of C₃H₃N₂CH₂NC₃H₃NC(CH₃)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=(C₃H₃N₂CH₂NC₃H₃NC(CH₃)3)B(C₆H₅)4

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Technology Process of C₃H₃N₂CH₂NC₃H₃NC(CH₃)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=(C₃H₃N₂CH₂NC₃H₃NC(CH₃)3)B(C₆H₅)4

There total 1 articles about C₃H₃N₂CH₂NC₃H₃NC(CH₃)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=(C₃H₃N₂CH₂NC₃H₃NC(CH₃)3)B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 143-66-8
sodium tetraphenyl borate

: 73901-67-4
1-(chloromethyl)pyrazole hydrochloride

: 45676-04-8
1-tert-butylimidazole

: 1191987-61-7
C₃H₃N₂CH₂NC₃H₃NC(CH₃)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=(C₃H₃N₂CH₂NC₃H₃NC(CH₃)3)B(C₆H₅)4

Guidance literature:: 1-(chloromethyl)pyrazole hydrochloride; 1-tert-butylimidazole; In toluene; for 2h; Reflux;

sodium tetraphenyl borate; In toluene; at 20 ℃; for 1.08333h; Reflux;
DOI:10.1039/b906724h

Reference yield: 71.0%

: methoxy(cyclooctadiene)rhodium(I) dimer

: 75-09-2
dichloromethane

: 1191987-61-7
C₃H₃N₂CH₂NC₃H₃NC(CH₃)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=(C₃H₃N₂CH₂NC₃H₃NC(CH₃)3)B(C₆H₅)4

: [Rh(C₃H₃N₂CH₂NC₃H₂N-t-Bu)(1,5-cyclooctadiene)]BPh₄*0.5CH₂Cl₂

Guidance literature:: With NaOMe; In methanol; under N2; freshly prepared soln. of NaOMe in MeOH filtered into MeOH soln. of Rh complex and pyrazolyl-imidazolium salt; refluxed for several h;cooled to room temp.; vol. reduced under vac.; filtered; ppt. washed with Et2O; dried in vac.;recrystd. from CH2Cl2-hexane; elem. anal.;
DOI:10.1039/b906724h