1-Methoxy-2-methyl-4-nitrosobenzene

Base Information

Chemical Name:1-Methoxy-2-methyl-4-nitrosobenzene
CAS No.:125708-82-9
Molecular Formula:C8H9NO2
Molecular Weight:151.165
Hs Code.:
DSSTox Substance ID:DTXSID90559976
Nikkaji Number:J618.538J
Wikidata:Q82442899
Mol file:125708-82-9.mol

Synonyms:1-Methoxy-2-methyl-4-nitrosobenzene;125708-82-9;2-Methyl-4-nitrosoanisole;DTXSID90559976

Suppliers and Price of 1-Methoxy-2-methyl-4-nitrosobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-Methoxy-2-methyl-4-nitrosobenzene

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:151.063328530
Heavy Atom Count:11
Complexity:138

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)N=O)OC

Technology Process of 1-Methoxy-2-methyl-4-nitrosobenzene

There total 4 articles about 1-Methoxy-2-methyl-4-nitrosobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 578-58-5
2-methylmethoxybenzene

: 125708-82-9
1-methoxy-2-methyl-4-nitrosobenzene

Guidance literature:: With nitrosylsulfuric acid; sulfuric acid; acetic acid; at 0 ℃; for 0.0666667h;

Reference yield:

: 14786-82-4
4-hydroxy-2-methylanisole

: 125708-82-9
1-methoxy-2-methyl-4-nitrosobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: [bis(acetoxy)iodo]benzene / 0 - 20 °C / Inert atmosphere

2: pyridine; hydroxyammonium sulfate / methanol / 20 °C / Inert atmosphere

With pyridine; hydroxyammonium sulfate; [bis(acetoxy)iodo]benzene; In methanol;
DOI:10.1039/c6ob00073h

Reference yield:

: 108-39-4
3-methyl-phenol

: 125708-82-9
1-methoxy-2-methyl-4-nitrosobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: [bis(acetoxy)iodo]benzene / 0.53 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h / 0 - 20 °C / Inert atmosphere

2.1: [bis(acetoxy)iodo]benzene / 0 - 20 °C / Inert atmosphere

3.1: pyridine; hydroxyammonium sulfate / methanol / 20 °C / Inert atmosphere

With pyridine; hydroxyammonium sulfate; [bis(acetoxy)iodo]benzene; In methanol;
DOI:10.1039/c6ob00073h