(CO)5W{μ2-(Ph)vinylphosphido}Fe(CO)2(cyclopentadienyl)

Base Information

Chemical Name:(CO)5W{μ2-(Ph)vinylphosphido}Fe(CO)2(cyclopentadienyl)
CAS No.:112712-71-7
Molecular Formula:C₂₀H₁₃FeO₇PW
Molecular Weight:635.99
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CO)5W{μ2-(Ph)vinylphosphido}Fe(CO)2(cyclopentadienyl)

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Technology Process of (CO)5W{μ2-(Ph)vinylphosphido}Fe(CO)2(cyclopentadienyl)

There total 3 articles about (CO)5W{μ2-(Ph)vinylphosphido}Fe(CO)2(cyclopentadienyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 101078-19-7
((phenyl)(vinyl)chlorophosphine)W(CO)5

: 112712-71-7
(CO)5W{μ2-(Ph)vinylphosphido}Fe(CO)2(cyclopentadienyl)

Guidance literature:: In toluene; heating of the W compd. and the Fe compd. in toluene with stirring to 110°C for 1h under oxygen-free Ar; filtn., evapn. (vacuum), chromy. (elution with hexane-toluene) and recrystn. from hexane-toluene; elem. anal.;
DOI:10.1021/om00094a027

Reference yield:

: 101144-76-7
{η3-(carbonyl)5tungstenP(Ph)(CHCH2)}iron(carbonyl)(cyclopentadienyl)

: 112712-71-7
(CO)5W{μ2-(Ph)vinylphosphido}Fe(CO)2(cyclopentadienyl)

Guidance literature:: With carbon monoxide; In toluene; heating of the W complex in toluene for 1 h at 100°C with CO (autoclave, 5 atm); cooling to room temp., removing the solvent and chromy.;
DOI:10.1021/om00094a027