2-methyl-2-phenyl-1,3,6-trithia-2-stannocane

Base Information

Chemical Name:2-methyl-2-phenyl-1,3,6-trithia-2-stannocane
CAS No.:78888-00-3
Molecular Formula:C₁₁H₁₆S₃Sn
Molecular Weight:363.156
Hs Code.:

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Chemical Property of 2-methyl-2-phenyl-1,3,6-trithia-2-stannocane

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Technology Process of 2-methyl-2-phenyl-1,3,6-trithia-2-stannocane

There total 2 articles about 2-methyl-2-phenyl-1,3,6-trithia-2-stannocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 15649-26-0
methylphenyltin(IV) dichloride

: bis-2-mercaptoethyl sulfide, disodium salt

: 78888-00-3
2-methyl-2-phenyl-1,3,6-trithia-2-stannocane

Guidance literature:: In ethanol; benzene; dithiolate in ethanol and MePhSnCl2 in benzene were added dropwise to boiling benzene with vigorous stirring, refluxed (12 h); hot soln. was filtered, solvent evapd., repptd. (petroleum ether, 100-140°C); elem. anal.;

Reference yield: 70.0%

: 3570-55-6
3-thiapentan-1,5-dithiol

: 15649-26-0
methylphenyltin(IV) dichloride

: 78888-00-3
2-methyl-2-phenyl-1,3,6-trithia-2-stannocane

Guidance literature:: With Na; In ethanol; benzene; (a) dithiol refluxed for 1 h with Na in EtOH, (b) added dropwise to boiling C6H6 with Sn educt soln. with stirring, refluxed for 4 h; filtered, concd., recrystd. from petroleum ether; elem. anal.;
DOI:10.1016/S0022-328X(00)81913-0