(cyclooctadienyl-pentafluorophenyl)PtI

Base Information

Chemical Name:(cyclooctadienyl-pentafluorophenyl)PtI
CAS No.:112100-79-5
Molecular Formula:C₁₄H₁₂F₅IPt
Molecular Weight:597.226
Hs Code.:

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Chemical Property of (cyclooctadienyl-pentafluorophenyl)PtI

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Technology Process of (cyclooctadienyl-pentafluorophenyl)PtI

There total 2 articles about (cyclooctadienyl-pentafluorophenyl)PtI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: chloro(η4-cis,cis-cycloocta-1,5-diene)pentafluorophenylplatinum(II)

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 112100-79-5
(cyclooctadienyl-pentafluorophenyl)PtI

Guidance literature:: In water; acetone; a soln. of Pt-complex in 1:2 v/v aq. acetone was stirred overnight withNaI; acetone was evapd. in vacuo, aq. suspn. was extd. with ether, ext. evapd., residue was crystd. from ether-petroleum ether; elem. anal.;
DOI:10.1016/0022-328X(87)85013-1

Reference yield: 34.0%

: 12266-72-7
(1,5-cylooctadiene)di-iodoplatinum(II)

: 344-04-7
bromopentafluorobenzene

: 112100-79-5
(cyclooctadienyl-pentafluorophenyl)PtI

Guidance literature:: With n-C₄H₉Li; In tetrahydrofuran; diethyl ether; hexane; (N2); C6F5Br in Et2O was treated with n-BuLi in hexane at -60°C, stirred for 10 min and then THF soln. of Pt compd. added; mixt. was warmed up to room temp. within 1 h; mixt. shaked with H2O, organic layer septd. and evapd. to dryness;

Reference yield: 94.0%

: 112100-79-5
(cyclooctadienyl-pentafluorophenyl)PtI

: 983-80-2
cis-1,2-bis-(diphenylphosphino)ethene

: 119325-75-6
(1,2-bis(diphenylphosphino)ethylene)Pt(C₆F₅)I

Guidance literature:: In benzene; (N2); to soln. of Pt compd. was added solid ligand and stirred at room temp. overnight; addn. of Et2O yielded white product, which was filtered, washed with Et2O and recrystd. from CH2Cl2/MeOH; elem. anal.;