Technology Process of 1-Allyl-4-benzyloxy-5-methoxy-6-methyl-1H-indole-2-carbaldehyde
There total 10 articles about 1-Allyl-4-benzyloxy-5-methoxy-6-methyl-1H-indole-2-carbaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 97 percent / H(1+)
2: 76 percent / TiCl4 / CH2Cl2 / 0 °C
3: 78 percent / NaH / dimethylformamide
4: 1.) m-chloroperbenzoic acid; 2.) HCl, H2O / 1.) CH2Cl2; 2.) CH3OH
5: 71 percent / K2CO3 / acetone
6: 1.) LiAlH4; 2.) BaMnO4 / 1.) ether; 2.) CH2Cl2
7: sodium methoxide / methanol / -15 °C
8: xylene / Heating
9: 99 percent / LiAlH4 / diethyl ether
10: 69 percent / BaMnO4 / CH2Cl2
11: 80 percent / NaH / dimethylformamide
With
hydrogenchloride; lithium aluminium tetrahydride; barium permanganate; water; sodium methylate; hydrogen cation; titanium tetrachloride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; xylene;
DOI:10.1039/c39890000186
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 76 percent / TiCl4 / CH2Cl2 / 0 °C
2: 78 percent / NaH / dimethylformamide
3: 1.) m-chloroperbenzoic acid; 2.) HCl, H2O / 1.) CH2Cl2; 2.) CH3OH
4: 71 percent / K2CO3 / acetone
5: 1.) LiAlH4; 2.) BaMnO4 / 1.) ether; 2.) CH2Cl2
6: sodium methoxide / methanol / -15 °C
7: xylene / Heating
8: 99 percent / LiAlH4 / diethyl ether
9: 69 percent / BaMnO4 / CH2Cl2
10: 80 percent / NaH / dimethylformamide
With
hydrogenchloride; lithium aluminium tetrahydride; barium permanganate; water; sodium methylate; titanium tetrachloride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; xylene;
DOI:10.1039/c39890000186
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 78 percent / NaH / dimethylformamide
2: 1.) m-chloroperbenzoic acid; 2.) HCl, H2O / 1.) CH2Cl2; 2.) CH3OH
3: 71 percent / K2CO3 / acetone
4: 1.) LiAlH4; 2.) BaMnO4 / 1.) ether; 2.) CH2Cl2
5: sodium methoxide / methanol / -15 °C
6: xylene / Heating
7: 99 percent / LiAlH4 / diethyl ether
8: 69 percent / BaMnO4 / CH2Cl2
9: 80 percent / NaH / dimethylformamide
With
hydrogenchloride; lithium aluminium tetrahydride; barium permanganate; water; sodium methylate; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; xylene;
DOI:10.1039/c39890000186
