C₃₀H₃₁NO₂

Base Information

Chemical Name:C₃₀H₃₁NO₂
CAS No.:1351204-66-4
Molecular Formula:C₃₀H₃₁NO₂
Molecular Weight:437.582
Hs Code.:

C<sub>30</sub>H<sub>31</sub>NO<sub>2</sub>

Synonyms:

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Chemical Property of C₃₀H₃₁NO₂

Chemical Property:

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Technology Process of C₃₀H₃₁NO₂

There total 6 articles about C₃₀H₃₁NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3335-95-3
N-benzyl-3-phenyl-2-oxindole

: (propa-1,2-dien-1-yloxy)cyclohexane

: 1351204-66-4
C₃₀H₃₁NO₂

: C₃₀H₃₁NO₂

: C₃₀H₃₁NO₂

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; benzoic acid; In tetrahydrofuran; at 20 ℃; for 14h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja209244m

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1351204-66-4
C₃₀H₃₁NO₂

: C₃₀H₃₁NO₂

: C₃₀H₃₁NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: acetic acid; tin(ll) chloride / 4 h / 80 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; benzoic acid / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; acetic acid; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; benzoic acid; tin(ll) chloride; In tetrahydrofuran;
DOI:10.1021/ja209244m

Reference yield:

: 108-93-0
cyclohexanol

: 1351204-66-4
C₃₀H₃₁NO₂

: C₃₀H₃₁NO₂

: C₃₀H₃₁NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

1.2: 3 h / 0 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; benzoic acid / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium tert-butylate; sodium hydride; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; benzoic acid; In tetrahydrofuran; mineral oil;
DOI:10.1021/ja209244m