C₄H₁₁N*C₃₀H₃₂N₆O₆

Base Information

Chemical Name:C₄H₁₁N*C₃₀H₃₂N₆O₆
CAS No.:1360054-67-6
Molecular Formula:C₄H₁₁N*C₃₀H₃₂N₆O₆
Molecular Weight:645.759
Hs Code.:

C<sub>4</sub>H<sub>11</sub>N*C<sub>30</sub>H<sub>32</sub>N<sub>6</sub>O<sub>6</sub>

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Chemical Property of C₄H₁₁N*C₃₀H₃₂N₆O₆

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Technology Process of C₄H₁₁N*C₃₀H₃₂N₆O₆

There total 9 articles about C₄H₁₁N*C₃₀H₃₂N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 264608-14-2
2-chloro-N-(2,2-diphenylethyl)-9-(tetrahydro-2H-pyran-2-yl)-9H-purin-6-amine

: 1360054-67-6
C₄H₁₁N*C₃₀H₃₂N₆O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium carbonate / 105 °C / 15001.5 Torr / Autoclave

2.1: trifluoroacetic acid / ethanol / 20 h / 50 °C / Inert atmosphere

3.1: 4-methyl-morpholine / 1,2-dimethoxyethane / 50 - 60 °C / Inert atmosphere; Large scale reaction

4.1: 1,2-dimethoxyethane / 1.75 h / 65 °C / Inert atmosphere; Large scale reaction

5.1: ethanol; 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 °C / Inert atmosphere

6.1: sulfuric acid / acetone / 0.83 h / 20 °C / Inert atmosphere; Large scale reaction

7.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetraethylammonium bromide; sodium hydrogencarbonate / dichloromethane / 2 - 5 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: dichloromethane / 20 °C / Inert atmosphere; Large scale reaction

9.1: dichloromethane / -15 - 0 °C / Inert atmosphere

10.1: sodium hydroxide / methanol; water / 5 - 40 °C / Inert atmosphere; Large scale reaction

10.2: pH 1 - 2 / Inert atmosphere; Large scale reaction

11.1: Isopropyl acetate; water / Inert atmosphere; Large scale reaction

With 4-methyl-morpholine; 1,1'-bis-(diphenylphosphino)ferrocene; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; sulfuric acid; tetraethylammonium bromide; palladium diacetate; sodium hydrogencarbonate; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; sodium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; Isopropyl acetate; water; acetone;
DOI:10.1021/op200365n

Reference yield:

: ethyl 6-[(2,2-diphenylethyl)amino]-9H-purine-2-carboxylate

: 1360054-67-6
C₄H₁₁N*C₃₀H₃₂N₆O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: 4-methyl-morpholine / 1,2-dimethoxyethane / 50 - 60 °C / Inert atmosphere; Large scale reaction

2.1: 1,2-dimethoxyethane / 1.75 h / 65 °C / Inert atmosphere; Large scale reaction

3.1: ethanol; 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 °C / Inert atmosphere

4.1: sulfuric acid / acetone / 0.83 h / 20 °C / Inert atmosphere; Large scale reaction

5.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetraethylammonium bromide; sodium hydrogencarbonate / dichloromethane / 2 - 5 °C / Inert atmosphere

5.2: Inert atmosphere

6.1: dichloromethane / 20 °C / Inert atmosphere; Large scale reaction

7.1: dichloromethane / -15 - 0 °C / Inert atmosphere

8.1: sodium hydroxide / methanol; water / 5 - 40 °C / Inert atmosphere; Large scale reaction

8.2: pH 1 - 2 / Inert atmosphere; Large scale reaction

9.1: Isopropyl acetate; water / Inert atmosphere; Large scale reaction

With 4-methyl-morpholine; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; sulfuric acid; tetraethylammonium bromide; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; In methanol; 1,2-dimethoxyethane; dichloromethane; Isopropyl acetate; water; acetone;
DOI:10.1021/op200365n

Reference yield:

: C₃₃H₃₃N₇O₆

: 1360054-67-6
C₄H₁₁N*C₃₀H₃₂N₆O₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / -15 - 0 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 5 - 40 °C / Inert atmosphere; Large scale reaction

2.2: pH 1 - 2 / Inert atmosphere; Large scale reaction

3.1: Isopropyl acetate; water / Inert atmosphere; Large scale reaction

With sodium hydroxide; In methanol; dichloromethane; Isopropyl acetate; water;
DOI:10.1021/op200365n