ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate

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Chemical Name:ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate
CAS No.:313345-14-1
Molecular Formula:C₂₇H₂₉N₅O₃
Molecular Weight:471.559
Hs Code.:

Synonyms:ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate

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Chemical Property of ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate

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Technology Process of ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate

There total 2 articles about ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 264608-14-2
2-chloro-N-(2,2-diphenylethyl)-9-(tetrahydro-2H-pyran-2-yl)-9H-purin-6-amine

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 313345-14-1
ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium carbonate; at 105 ℃; under 15001.5 Torr; Autoclave;
DOI:10.1021/op200365n

Reference yield:

: 264608-14-2
2-chloro-N-(2,2-diphenylethyl)-9-(tetrahydro-2H-pyran-2-yl)-9H-purin-6-amine

: 313345-14-1
ethyl 6-[(2,2-diphenylethyl)amino]-9-(tetrahydro-2H-pyran-2-yl)-9H-purine-2-carboxylate

Guidance literature:: 2-chloro-N-(2,2-diphenylethyl)-9-(tetrahydro-2H-pyran-2-yl)-9H-purin-6-amine; With carbon monoxide; triethylamine; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; In ethanol; at 0 - 120 ℃; for 20h; under 12938.8 Torr;

In ethyl acetate; at 20 ℃; for 60h;