trans-dinitratodiaquapalladium(II)

Base Information

Chemical Name:trans-dinitratodiaquapalladium(II)
CAS No.:1147543-08-5
Molecular Formula:H₄N₂O₈Pd
Molecular Weight:266.46
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-dinitratodiaquapalladium(II)

Chemical Property:

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Technology Process of trans-dinitratodiaquapalladium(II)

There total 1 articles about trans-dinitratodiaquapalladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7732-18-5
water

: 7697-37-2,78989-43-2
nitric acid

: 7440-05-3
palladium

: 82279-70-7,1147543-08-5
trans-dinitratodiaquapalladium(II)

Guidance literature:: With HCl; In nitric acid; aq. HNO3; Pd powder dissolved at 90-95°C within 1 h in HNO3 (d. 1.419 g/ml)with addn. of HCl (d. 1.165 g/ml), then soln. evapd. at the same temp., diluted with water; concd. in air to wet crystals, dried in desiccator for 1-2 d over KOH; elem. anal.;
DOI:10.1134/S1070427207050023

Reference yield: 85.0%

: 82279-70-7,1147543-08-5
trans-dinitratodiaquapalladium(II)

: 64-19-7,77671-22-8
acetic acid

: 3375-31-3
palladium diacetate

Guidance literature:: In acetic acid; Pd(II) nitrate dissolved in anhyd. acetic acid; stirred for 3 h at room temp.; suspn. diluted with acetic acid; centrifuged; washed (H2O, acetone); dried (vac., NaOH); elem. anal.;
DOI:10.1134/S003602361110024X

Reference yield: 61.0%

: 82279-70-7,1147543-08-5
trans-dinitratodiaquapalladium(II)

: 64-19-7,77671-22-8
acetic acid

: palladium (II) acetate

: 3375-31-3
palladium diacetate

Guidance literature:: In water; acetic acid; Pd(II) nitrate dissolved in mixt. of acetic acid and H2O; mixt. stirred for 3 h at room temp.; filtered; washed (glacial acetic acid, ether); dried (vac. over alkali);mixt. extd. (benzene); filtered; filtrate evapd. to dryness at 40.degre e.C in vac.; elem. anal.;
DOI:10.1134/S003602361110024X