CoBu(pyridine)(dithiophenylglyoxime(-1H))2

Base Information

Chemical Name:CoBu(pyridine)(dithiophenylglyoxime(-1H))2
CAS No.:1159404-42-8
Molecular Formula:C₃₇H₃₆CoN₅O₄S₄
Molecular Weight:801.981
Hs Code.:

Synonyms:

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Chemical Property of CoBu(pyridine)(dithiophenylglyoxime(-1H))2

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Technology Process of CoBu(pyridine)(dithiophenylglyoxime(-1H))2

There total 3 articles about CoBu(pyridine)(dithiophenylglyoxime(-1H))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1313442-69-1
CoCl(pyridine)(dithiophenylglyoxime(-1H))(dimethylglyoxime(-1H))

: 1313442-72-6
CoBu(pyridine)(dithiophenylglyoxime(-1H))(dimethylglyoxime(-1H))

: 1159404-42-8
CoBu(pyridine)(dithiophenylglyoxime(-1H))2

Guidance literature:: With NaBH₄; In not given; reacted for 15 min;
DOI:10.1016/j.jorganchem.2011.02.033

Reference yield:

: 1159404-38-2
CoCl((bis(thiophenyl)glyoxime-H)2(pyridine)

: 1159404-42-8
BuCo((bis(thiophenyl)glyoxime-H)2(pyridine)

Guidance literature:: With NaOH; sodium borohydride; In ethanol; soln. of Co compd. in EtOH purged (N2, 10 min), cooled (0°C, stirring), aq. solns. of NaOH and NaBH4 added, soln. of butyl halide in EtOHadded, mixt. stirred (0°C, 1 h), concd. under vac., poured into H20 contg. some drops of pyridine; ppt. filtered off, washed with H2O and dried, column chromy. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1021/om900065k

Reference yield:

: 110-86-1
pyridine

: 1313442-72-6
CoBu(pyridine)(dithiophenylglyoxime(-1H))(dimethylglyoxime(-1H))

: 1159404-42-8
CoBu(pyridine)(dithiophenylglyoxime(-1H))2

Guidance literature:: Multi-step reaction with 2 steps

1: air / ethanol

2: NaBH₄ / not given

With air; NaBH₄; In ethanol;
DOI:10.1016/j.jorganchem.2011.02.033