tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane

Base Information

Chemical Name:tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane
CAS No.:957878-46-5
Molecular Formula:C₄₁H₅₄Ge₂O₂
Molecular Weight:724.059
Hs Code.:

Synonyms:

Suppliers and Price of tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane

There total 6 articles about tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: (1,3-diisoproyl-4,5-dimethylimidazolin-2-ylidene)bis(2,4,6-trimethylphenyl)germanium(II)

: 75-98-9
Trimethylacetic acid

: 957878-46-5
tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane

Guidance literature:: In tetrahydrofuran; under N2, Schlenk techniques; dropwise addn. of soln. of pivalic acid inTHF to soln. of Ge compd. in THF; evapn. under vac., residue suspended in Et2O, extn. with aq. NH4Cl, org.phase sepd. and dried over MgSO4, filtration, filtrate evapd. under vac .;
DOI:10.1021/om100059z

Reference yield: 53.0%

: 115385-07-4
tetrakis(2,4,6-trimethylphenyl)digermene

: 75-98-9
Trimethylacetic acid

: 154079-41-1
(hydroxydimesitylgermyl)dimesitylgermane

: 957878-46-5
tetrakis(2,4,6-trimethylphenyl)(tert-butylcarbonyloxy)digermane

Guidance literature:: In tetrahydrofuran; (N2); dissolving of soln. of pivalic acid in THF; addn. to soln. of (mesityl)4Ge2 in THF for 5 min at room temp.; removal of solvent by rotary evapn.; chromy. (silica gel; 70/30 CH2Cl2/hexanes);
DOI:10.1021/om7005358