[Pb(benzene-1,3-dicarboxylato)(dipyrido[3,2-a:2',3'-c]-phenazine)] monohydrate

Base Information

• Chemical Name: [Pb(benzene-1,3-dicarboxylato)(dipyrido[3,2-a:2',3'-c]-phenazine)] monohydrate
• CAS No.: 947503-69-7
• Molecular Formula: C₈H₄O₄*C₁₈H₁₀N₄*H₂O*Pb
• Molecular Weight: 671.637
• Mol file: 947503-69-7.mol

Synonyms:

Chemical Property of [Pb(benzene-1,3-dicarboxylato)(dipyrido[3,2-a:2',3'-c]-phenazine)] monohydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pb(benzene-1,3-dicarboxylato)(dipyrido[3,2-a:2',3'-c]-phenazine)] monohydrate

There total 1 articles about [Pb(benzene-1,3-dicarboxylato)(dipyrido[3,2-a:2',3'-c]-phenazine)] monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

dipyridil[3,2-a:2',3'-c]phenazine (19535-47-8) + lead(II) nitrate + isophthalic acid (121-91-5) + water (7732-18-5) → [Pb(benzene-1,3-dicarboxylato)(dipyrido[3,2-a:2',3'-c]-phenazine)] monohydrate (947503-69-7)

Guidance literature:

With Et₃N; In water; High Pressure; under hydrothermal conditions; Et3N added to mixt. of Pb(NO3)2 and two ligands in distd. H2O (pH 5-6); heated in stainless steel autoclave at 170°C for 4 d; cooled slowly to room temp.; filtered; crystals washed with distd. H2O; dried in air at ambient temp.; elem. anal.;

DOI:10.1021/ic700613c

upstream raw materials:

dipyridil[3,2-a:2',3'-c]phenazine

isophthalic acid

water