C₄₈H₆₆N₄O₃

Base Information

Chemical Name:C₄₈H₆₆N₄O₃
CAS No.:110589-05-4
Molecular Formula:C₄₈H₆₆N₄O₃
Molecular Weight:747.077
Hs Code.:

C<sub>48</sub>H<sub>66</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₄₈H₆₆N₄O₃

Chemical Property:

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Technology Process of C₄₈H₆₆N₄O₃

There total 12 articles about C₄₈H₆₆N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6327-85-1
2,6-bis(hydroxymethyl)-4-methyl-anisole

: 110589-05-4
C₄₈H₆₆N₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) DMSO/(COCl)2, 2.) Et₃N / 1.) methylene chloride, -78 deg C, 15 min, 2.) methylene chloride, from -78 deg C to RT

2: 60.4 percent / K₂CO₃ / dioxane / 44 h / Heating

3: 96.7 percent / H₂,Et₃N / 10percent Pd/C / tetrahydrofuran / 24 h / Ambient temperature

4: 85.2 percent / glacial acetic acid / 1 h / 80 °C

5: KOH/H₂O / propan-1-ol / 3 h / Heating

6: DMF / 3 h / Heating

With potassium hydroxide; oxalyl dichloride; water; hydrogen; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; propan-1-ol;
DOI:10.1021/jo00233a011

Reference yield:

: 71128-83-1
2-methoxy-5-methyl-1,3-benzenedicarboxaldehyde

: 110589-05-4
C₄₈H₆₆N₄O₃

Guidance literature:: Multi-step reaction with 5 steps

1: 60.4 percent / K₂CO₃ / dioxane / 44 h / Heating

2: 96.7 percent / H₂,Et₃N / 10percent Pd/C / tetrahydrofuran / 24 h / Ambient temperature

3: 85.2 percent / glacial acetic acid / 1 h / 80 °C

4: KOH/H₂O / propan-1-ol / 3 h / Heating

5: DMF / 3 h / Heating

With potassium hydroxide; water; hydrogen; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; propan-1-ol;
DOI:10.1021/jo00233a011

Reference yield:

: 98977-15-2
5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-1-iodopentane

: 110589-05-4
C₄₈H₆₆N₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1: 96.6 percent / toluene / 25 h / Heating

2: 60.4 percent / K₂CO₃ / dioxane / 44 h / Heating

3: 96.7 percent / H₂,Et₃N / 10percent Pd/C / tetrahydrofuran / 24 h / Ambient temperature

4: 85.2 percent / glacial acetic acid / 1 h / 80 °C

5: KOH/H₂O / propan-1-ol / 3 h / Heating

6: DMF / 3 h / Heating

With potassium hydroxide; water; hydrogen; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; propan-1-ol; toluene;
DOI:10.1021/jo00233a011