Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 3-methyl-

Base Information

Chemical Name:Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 3-methyl-
CAS No.:126889-61-0
Molecular Formula:C9H8O
Molecular Weight:132.162
Hs Code.:
DSSTox Substance ID:DTXSID30372929
Nikkaji Number:J452.687B
Wikidata:Q82160928
Mol file:126889-61-0.mol

Synonyms:126889-61-0;Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 3-methyl-;SCHEMBL19068618;DTXSID30372929;AKOS004907546;3-Methylbicyclo[4.2.0]octa-1,3,5-trien-7-one

Suppliers and Price of Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 3-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 3-methyl-

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:132.057514874
Heavy Atom Count:10
Complexity:162

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)C(=O)C2

Technology Process of Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 3-methyl-

There total 2 articles about Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 126889-58-5
2-(1'-Hydroxy-1',2'-dihydro-4'-methylbenzocyclobuten-1'-yl)-2,4-dimethylpentan-3-one

: 126889-61-0
4-methylbenzocyclobuten-1(2H)-one

: 565-80-0
2,4-dimethylpentan-3-one

Guidance literature:: at 150 ℃; for 3h; under 760 Torr;

Reference yield:

: 108-31-6
maleic anhydride

: 91416-35-2
(4-Methyl-6-methylene-cyclohexa-2,4-dienylidene)-methanone

: 23617-71-2
2,4-dimethyl-benzoic acid methyl ester

: 126889-61-0
4-methylbenzocyclobuten-1(2H)-one

: 7-Methyl-9,9a-dihydro-3aH-naphtho[2,3-c]furan-1,3,4-trione

Guidance literature:: In diethyl ether; at 23 ℃; Title compound not separated from byproducts; Irradiation;
DOI:10.1016/S0040-4039(01)80210-0

Reference yield: 83.0%

: 24395-14-0
N-(p-tolylsulfonyl)-2-phenylaziridine

: 126889-61-0
4-methylbenzocyclobuten-1(2H)-one

: C₂₄H₂₃NO₃S

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; 2-[4,5-dihydro-1,3-oxazol-2-yl]pyridine; In acetonitrile; at 60 ℃; for 12h;
DOI:10.1038/s41557-021-00746-7