Ethanone, 1-[7,8-dihydro-8-(4-hydroxy-3,5-dimethoxyphenyl)-6-methoxy-6-methyl-6 H-1,3-dioxolo[4,5-g][1]benzopyran-7-yl]-

Base Information

Chemical Name:Ethanone, 1-[7,8-dihydro-8-(4-hydroxy-3,5-dimethoxyphenyl)-6-methoxy-6-methyl-6 H-1,3-dioxolo[4,5-g][1]benzopyran-7-yl]-
CAS No.:126935-01-1
Molecular Formula:C₂₂H₂₄O₈
Molecular Weight:416.428
Hs Code.:
Mol file:126935-01-1.mol

Synonyms:

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Chemical Property of Ethanone, 1-[7,8-dihydro-8-(4-hydroxy-3,5-dimethoxyphenyl)-6-methoxy-6-methyl-6 H-1,3-dioxolo[4,5-g][1]benzopyran-7-yl]-

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Technology Process of Ethanone, 1-[7,8-dihydro-8-(4-hydroxy-3,5-dimethoxyphenyl)-6-methoxy-6-methyl-6 H-1,3-dioxolo[4,5-g][1]benzopyran-7-yl]-

There total 3 articles about Ethanone, 1-[7,8-dihydro-8-(4-hydroxy-3,5-dimethoxyphenyl)-6-methoxy-6-methyl-6 H-1,3-dioxolo[4,5-g][1]benzopyran-7-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126935-00-0
NCI 369077

: 126935-01-1
1-[(7R,8R)-8-(4-Hydroxy-3,5-dimethoxy-phenyl)-6-methoxy-6-methyl-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromen-7-yl]-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 5.2 g / H₂O; acetic acid / 0.17 h / Heating

2: 1.0 g / conc. HCl

With hydrogenchloride; In water; acetic acid;
DOI:10.1002/jhet.5570260524

Reference yield:

: 134-96-3
syringic aldehyde

: 126935-01-1
1-[(7R,8R)-8-(4-Hydroxy-3,5-dimethoxy-phenyl)-6-methoxy-6-methyl-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromen-7-yl]-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / methanol / 3 h / Heating

2: 5.2 g / H₂O; acetic acid / 0.17 h / Heating

3: 1.0 g / conc. HCl

With hydrogenchloride; In methanol; water; acetic acid;
DOI:10.1002/jhet.5570260524