C₂₀H₂₅N₃O₃

Base Information

Chemical Name:C₂₀H₂₅N₃O₃
CAS No.:1346515-36-3
Molecular Formula:C₂₀H₂₅N₃O₃
Molecular Weight:355.437
Hs Code.:

C<sub>20</sub>H<sub>25</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₅N₃O₃

Chemical Property:

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Technology Process of C₂₀H₂₅N₃O₃

There total 4 articles about C₂₀H₂₅N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 954236-44-3
tert-butyl 3-oxo-1-oxa-8-azaspiro[4.5]decane-8-carboxylate

: 1346515-36-3
C₂₀H₂₅N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / methanol / 0 °C

2: carbon tetrabromide; triphenylphosphine / tetrahydrofuran

3: nickel(II) iodide; lithium hexamethyldisilazane / isopropyl alcohol

4: hydrogenchloride / 1,4-dioxane; dichloromethane

5: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

With nickel(II) iodide; hydrogenchloride; sodium tetrahydroborate; carbon tetrabromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; isopropyl alcohol; acetonitrile; 3: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.08.048

Reference yield:

: 240401-09-6
tert-butyl 3-hydroxy-1-oxa-8-azaspiro[ 4.5]decane-8-carboxylate

: 1346515-36-3
C₂₀H₂₅N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran

2: nickel(II) iodide; lithium hexamethyldisilazane / isopropyl alcohol

3: hydrogenchloride / 1,4-dioxane; dichloromethane

4: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

With nickel(II) iodide; hydrogenchloride; carbon tetrabromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; dichloromethane; isopropyl alcohol; acetonitrile; 2: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.08.048

Reference yield:

: 898157-46-5
tert-butyl 3-bromo-1-oxa-8-azaspiro[4.5]decane-8-carboxylate

: 1346515-36-3
C₂₀H₂₅N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: nickel(II) iodide; lithium hexamethyldisilazane / isopropyl alcohol

2: hydrogenchloride / 1,4-dioxane; dichloromethane

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

With nickel(II) iodide; hydrogenchloride; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; In 1,4-dioxane; dichloromethane; isopropyl alcohol; acetonitrile; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.08.048