bis[2,4,6-tribromophenoxy]triphenylantimony

Base Information

Chemical Name:bis[2,4,6-tribromophenoxy]triphenylantimony
CAS No.:102052-18-6
Molecular Formula:C₃₀H₁₉Br₆O₂Sb
Molecular Weight:1012.65
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[2,4,6-tribromophenoxy]triphenylantimony

Chemical Property:

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Technology Process of bis[2,4,6-tribromophenoxy]triphenylantimony

There total 3 articles about bis[2,4,6-tribromophenoxy]triphenylantimony which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1538-59-6,20265-30-9,34716-92-2
triphenylantimony dibromide

: 118-79-6
2,4,6-tribromophenol

: 102052-18-6
di(2,4,6-tribromophenolato)triphenylantimony(V)

Guidance literature:: With triethylamine; In benzene; byproducts: triethylamine hydrobromide; 2 equiv. Br3C6H2OH are stirred in dry benzene at 25-30°C for about 1 h, the mixt. was refluxed for about 2 h; triethylamine hydrobromide was filtered off, the filtrate was concd., petroleum ether was added, recrystd.(benzene/petroleum ether); elem. anal.;

Reference yield: 70.1%

: 1538-59-6,20265-30-9,34716-92-2
triphenylantimony dibromide

: 2666-53-7
sodium 2,4,6-tribromophenolate

: 102052-18-6
di(2,4,6-tribromophenolato)triphenylantimony(V)

Guidance literature:: In benzene; byproducts: NaBr; 2 equiv. Br3C6H2ONa are refluxed in dry benzene for about 4 h; NaBr was filtered off, the filtrate was concd., petroleum ether was added, recrystd. (benzene/petroleum ether); elem. anal.;

Reference yield: 47.0%

: 603-36-1
triphenylantimony

: 118-79-6
2,4,6-tribromophenol

: 102052-18-6
di(2,4,6-tribromophenolato)triphenylantimony(V)

Guidance literature:: With H₂O₂; In diethyl ether; water; aq. H2O2 added to mixt. of reagents in ether; crystd. for 12 h, crysts. filtered, recrystd. (toluene), dried;
DOI:10.1023/A:1016068409252