lκ-(2,3-di[1'2'7':η-2'-(diphenylmethylene)phenyl]quinoxaline-κN1,κN2)bis(tricarbonylmanganese(I))

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Chemical Name:lκ-(2,3-di[1'2'7':η-2'-(diphenylmethylene)phenyl]quinoxaline-κN1,κN2)bis(tricarbonylmanganese(I))
CAS No.:439684-67-0
Molecular Formula:C₅₂H₃₂Mn₂N₂O₆
Molecular Weight:890.712
Hs Code.:

Synonyms:

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Chemical Property of lκ-(2,3-di[1'2'7':η-2'-(diphenylmethylene)phenyl]quinoxaline-κN1,κN2)bis(tricarbonylmanganese(I))

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Technology Process of lκ-(2,3-di[1'2'7':η-2'-(diphenylmethylene)phenyl]quinoxaline-κN1,κN2)bis(tricarbonylmanganese(I))

There total 3 articles about lκ-(2,3-di[1'2'7':η-2'-(diphenylmethylene)phenyl]quinoxaline-κN1,κN2)bis(tricarbonylmanganese(I)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 439684-66-9
(2,3-(diphenyl-κC2',κC2'')quinoxaline-κN1,κN2)bis(tetracarbonylmanganese(I))

: 908093-98-1
diazodiphenylmethane

: 439684-67-0,1095001-50-5
(C₄H₄)(C₄N₂(C₆H₄C(C₆H₅)2)2)(Mn(CO)3)2

Guidance literature:: In n-heptane; toluene; manganese complexe reacts with Ph2CN2 in mixt. of boiling toluene and heptane; purified by chromy., recrystd.;
DOI:10.1039/b111570g

Reference yield: 60.0%

: 439684-66-9
(2,3-(diphenyl-κC2',κC2'')quinoxaline-κN1,κN2)bis(tetracarbonylmanganese(I))

: 908093-98-1
diazodiphenylmethane

: 1095001-50-5,439684-67-0
lκ-(2,3-di[1'2'7':η-2'-(diphenylmethylene)phenyl]quinoxaline-κN1,κN2)bis(tricarbonylmanganese(I))

Guidance literature:: In n-heptane; toluene; under Ar, refluxing with stirring for 30 min; soln. was cooled to room temp., solvent was evapd., mixt. was dissolved in CH2Cl2, SiO2 was added, solvent was evapd., residue was chromd., solvent was removed; elem. anal.;
DOI:10.1021/om020116z