p-chlorophenyl-β-cyanoethylphosphoric acid trimethylammonium salt

Base Information

Chemical Name:p-chlorophenyl-β-cyanoethylphosphoric acid trimethylammonium salt
CAS No.:78272-49-8
Molecular Formula:C₃H₉N*C₉H₉ClNO₄P
Molecular Weight:320.713
Hs Code.:

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Chemical Property of p-chlorophenyl-β-cyanoethylphosphoric acid trimethylammonium salt

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Technology Process of p-chlorophenyl-β-cyanoethylphosphoric acid trimethylammonium salt

There total 3 articles about p-chlorophenyl-β-cyanoethylphosphoric acid trimethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32666-92-5
p-chlorophenyl phosphorodichloridite

: 78272-49-8
p-chlorophenyl-β-cyanoethylphosphoric acid trimethylammonium salt

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylamine / benzene; diethyl ether / 0.5 h / -10 - 0 °C

2: tert-BuOOH / benzene / 1 h / 25 °C

3: acetonitrile / 1 h / Ambient temperature

With tert.-butylhydroperoxide; trimethylamine; In diethyl ether; acetonitrile; benzene;
DOI:10.1016/0040-4039(81)80013-5

Reference yield:

: 78272-46-5
p-chlorophenyl-bis-(β-cyanoethyl)-phosphite

: 78272-49-8
p-chlorophenyl-β-cyanoethylphosphoric acid trimethylammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: tert-BuOOH / benzene / 1 h / 25 °C

2: acetonitrile / 1 h / Ambient temperature

With tert.-butylhydroperoxide; In acetonitrile; benzene;
DOI:10.1016/0040-4039(81)80013-5