Fe(C₅H₄CO(CHCH)2C₆H₄N(CH₃)2)2

Base Information

• Chemical Name: Fe(C₅H₄CO(CHCH)2C₆H₄N(CH₃)2)2
• CAS No.: 900178-89-4
• Molecular Formula: C₃₆H₃₆FeN₂O₂
• Molecular Weight: 584.541

Synonyms:

Chemical Property of Fe(C₅H₄CO(CHCH)2C₆H₄N(CH₃)2)2

Chemical Property:

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Technology Process of Fe(C₅H₄CO(CHCH)2C₆H₄N(CH₃)2)2

There total 1 articles about Fe(C₅H₄CO(CHCH)2C₆H₄N(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1,1'-diacetylferrocene (1273-94-5) + p-dimethylaminocinnamaldehyde (6203-18-5) → Fe(C5H4CO(CHCH)2C6H4N(CH3)2)2 (900178-89-4)

Guidance literature:

With sodium hydroxide; In ethanol; (N2, Schlenk) a light-protected mixt. of complex, aldehyde and 1 equiv of NaOH was dissolved in ethanol, stirred for 4 h at room temp.; the mixt. was evapd. to dryness, column chromy. on dried silica, eluent 5:2 petroleum ether/ethyl acetate, THF, evapd. washed with pentane, dried; elem. anal.;

DOI:10.1021/ic060535e

Reference yield: 68.0%

tetrafluoroboric acid diethyl ether (67969-82-8) + Fe(C5H4CO(CHCH)2C6H4N(CH3)2)2 (900178-89-4) → Fe(C5H4CO(CHCH)2C6H4NH(CH3)2)2(2+)*2BF4(1-)=Fe(C5H4CO(CHCH)2C6H4NH(CH3)2)2(BF4)2

Guidance literature:

In acetonitrile; (N2, Schlenk) HBF4*Et2O was slowly added to a stirred soln. of complex in avetonitrile, the light-protected mixt. was stirred for 1 h; evapd., washed with ether and pentane, dried under vac.; elem. anal.;

DOI:10.1021/ic060535e

Reference yield:

Fe(C5H4CO(CHCH)2C6H4N(CH3)2)2 (900178-89-4) + calcium(II) trifluoromethanesulfonate (55120-75-7) → Fe(C5H4CO(CHCH)2C6H4N(CH3)2)2*2Ca(2+)

Guidance literature:

In [D₃]acetonitrile; (Ar, Schlenk) 2 equiv of Ca-salt, CD3CN; not sepd., detected by NMR spectra;

DOI:10.1021/ic060535e

upstream raw materials:

1,1'-diacetylferrocene

p-dimethylaminocinnamaldehyde

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