((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II)

Base Information

Chemical Name:((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II)
CAS No.:88867-61-2
Molecular Formula:C₂₅H₂₂AsCl₂PPt
Molecular Weight:694.331
Hs Code.:

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Chemical Property of ((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II)

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Technology Process of ((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II)

There total 3 articles about ((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 69783-37-5
<(Diphenylarsino)methyl>diphenylphosphan

: 88867-61-2
((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II)

Guidance literature:: In dichloromethane; soln. stirred for 1 h; the soln. was filtered, ether was added, the ppt. was filtered off, washed with ether, dried in vac., elem. anal.;

Reference yield: 21.0%

: 88867-59-8,88928-90-9
{cis-Cl₂(platinum)(mu.-(diphenylphosphino)(diphenylarsino)methane)2-trans-(rhodium)(CO)Cl}

: 69783-37-5
<(Diphenylarsino)methyl>diphenylphosphan

: 97112-55-5
RhCOCl((C₆H₅)4CH₂AsP)2PtCl₂

: 88867-61-2
((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II)

Guidance literature:: In dichloromethane; soln. of phosphine in CH2Cl2 was added to a soln. of complex in CH2Cl2;the mixt. was allowed to stand for 8 h; reduced in volume, MeOH was added, filtered off, filtrate was evapd., MeOH was added; recrystd. from CH2Cl2/Et2O;
DOI:10.1021/om00127a024

Reference yield: 19.0%

: 88867-59-8,88928-90-9
{cis-Cl₂(platinum)(mu.-(diphenylphosphino)(diphenylarsino)methane)2-trans-(rhodium)(CO)Cl}

: 97112-55-5
RhCOCl((C₆H₅)4CH₂AsP)2PtCl₂

: 88867-61-2
((diphenylphosphino)(diphenylarsino)methane)dichloroplatinum(II)

Guidance literature:: In chloroform; soln. of complex in chloroform was heated under reflux for 2 h; reduced in volume, MeOH was added dropwise, ppt. was filtered off; filtrate was evapd., MeOH was added; filtered, recrystd. from CH2Cl2/Et2O; vac.-dried; elem. anal.;
DOI:10.1021/om00127a024