C₄₀H₅₅N₉O₁₁S

Base Information

Chemical Name:C₄₀H₅₅N₉O₁₁S
CAS No.:1204332-52-4
Molecular Formula:C₄₀H₅₅N₉O₁₁S
Molecular Weight:869.996
Hs Code.:

C<sub>40</sub>H<sub>55</sub>N<sub>9</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₄₀H₅₅N₉O₁₁S

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Technology Process of C₄₀H₅₅N₉O₁₁S

There total 9 articles about C₄₀H₅₅N₉O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1204332-51-3
C₄₀H₅₇N₉O₁₂S

: 1204332-52-4
C₄₀H₅₅N₉O₁₁S

Guidance literature:: With 2,4,6-trimethyl-pyridine; 1-hydroxy-7-aza-benzotriazole; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200902398

Reference yield:

: 934612-57-4
Cbz-Arg(Mtr)-Gly-OMe

: 1204332-52-4
C₄₀H₅₅N₉O₁₁S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 20 % Pd(OH)2/C; hydrogen / methanol / 20 °C

2.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

4.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

5.1: titanium(IV) isopropylate / tetrahydrofuran / 20 h / 90 °C / Inert atmosphere; Molecular sieve

6.1: palladium on activated charcoal; hydrogen / methanol / 20 °C

7.1: 2,4,6-trimethyl-pyridine; 1-hydroxy-7-aza-benzotriazole; HATU / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; titanium(IV) isopropylate; 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; 20 % Pd(OH)2/C; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200902398

Reference yield:

: 934612-54-1
H₂N-L-Arg(Mtr)-Gly-OMe

: 1204332-52-4
C₄₀H₅₅N₉O₁₁S

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

3.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: titanium(IV) isopropylate / tetrahydrofuran / 20 h / 90 °C / Inert atmosphere; Molecular sieve

5.1: palladium on activated charcoal; hydrogen / methanol / 20 °C

6.1: 2,4,6-trimethyl-pyridine; 1-hydroxy-7-aza-benzotriazole; HATU / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; titanium(IV) isopropylate; 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200902398