N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide

Base Information

• Chemical Name: N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide
• CAS No.: 1085473-92-2
• Molecular Formula: C₁₉H₂₅N₃*HI
• Molecular Weight: 423.34
• Mol file: 1085473-92-2.mol

Synonyms:

Chemical Property of N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide

There total 2 articles about N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

S-methyl-N,N′-bis(2,6-dimethylphenyl)isothiourea hydroiodide (1085473-91-1) + dimethyl amine (124-40-3) → N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide (1085473-92-2)

Guidance literature:

In methanol; ethanol; at 70 ℃; for 7h; Sealed tube;

DOI:10.1021/ic302570s

Reference yield:

N,N′-bis(2,6-dimethylphenyl)thiourea (25480-78-8) → N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide (1085473-92-2)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 2 h / Reflux

2: methanol; ethanol / 7 h / 70 °C / Sealed tube

In methanol; ethanol;

DOI:10.1021/ic302570s

Reference yield:

N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidinium iodide (1085473-92-2) → N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidine (1085473-90-0)

Guidance literature:

With sodium carbonate; In diethyl ether; water; Saturated solution;

DOI:10.1021/ic302570s

upstream raw materials:

S-methyl-N,N′-bis(2,6-dimethylphenyl)isothiourea hydroiodide

dimethyl amine

N,N′-bis(2,6-dimethylphenyl)thiourea

Downstream raw materials:

N,N-dimethyl-N′,N″-bis(2,6-dimethylphenyl)guanidine