Technology Process of C28H34N8O8
There total 5 articles about C28H34N8O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-hydroxy-pyrrolidine-2,5-dione; 1,2-dichloro-ethane; triethylamine;
In
N,N-dimethyl-formamide;
at 50 ℃;
Inert atmosphere;
DOI:10.1021/cm403822w
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / tetrahydrofuran; toluene / 12 h / 0 - 20 °C / Inert atmosphere
2: dmap; triethylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere
3: sodium iodide / N,N-dimethyl-formamide / 80 °C
4: hydrazine hydrate; ethanol / Reflux
5: triethylamine; 1,2-dichloro-ethane; 1-hydroxy-pyrrolidine-2,5-dione / N,N-dimethyl-formamide / 50 °C / Inert atmosphere
With
dmap; 1-hydroxy-pyrrolidine-2,5-dione; ethanol; sodium hydride; hydrazine hydrate; 1,2-dichloro-ethane; triethylamine; sodium iodide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/cm403822w
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; triethylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere
2: sodium iodide / N,N-dimethyl-formamide / 80 °C
3: hydrazine hydrate; ethanol / Reflux
4: triethylamine; 1,2-dichloro-ethane; 1-hydroxy-pyrrolidine-2,5-dione / N,N-dimethyl-formamide / 50 °C / Inert atmosphere
With
dmap; 1-hydroxy-pyrrolidine-2,5-dione; ethanol; hydrazine hydrate; 1,2-dichloro-ethane; triethylamine; sodium iodide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/cm403822w
