N,1,1-triphenylphosphanecarboxamide sulfide

Base Information

Chemical Name:N,1,1-triphenylphosphanecarboxamide sulfide
CAS No.:10494-05-0
Molecular Formula:C₁₉H₁₆NOPS
Molecular Weight:337.382
Hs Code.:

Synonyms:Formanilide,1-(diphenylphosphinothioyl)- (7CI); Formanilide, 1-(diphenylthiophosphinyl)-(8CI); NSC 346107

Suppliers and Price of N,1,1-triphenylphosphanecarboxamide sulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N,1,1-triphenylphosphanecarboxamide sulfide

Chemical Property:

Density:1.27g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,1,1-triphenylphosphanecarboxamide sulfide

There total 2 articles about N,1,1-triphenylphosphanecarboxamide sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7067-72-3
N-Phenyl(diphenylphosphino)-formamid

: 10494-05-0
N-Phenyl(diphenylthiophosphoryl)-formamid

Guidance literature:: With sulfur; In ethanol; at 78 ℃;

Reference yield:

: 10494-05-0
N-Phenyl(diphenylthiophosphoryl)-formamid

Guidance literature:: Phosphin IV, S, Bzl.;

Reference yield: 46.0%

: 14100-30-2
pentacarbonylchloromanganese(I)

: 10494-05-0
N-Phenyl(diphenylthiophosphoryl)-formamid

: [(OC)4Mn-S=P(C₆H₅)2]2 (cyclo)

: tetracarbonyl-(diphenylthiophosphoryl-N-phenylformamido-N,S)-manganese

Guidance literature:: With triethylamine; In benzene; byproducts: CO, (C2H5)3HNCl, C6H5NCO; under N2, soln. of HN(Ph)C(O)P(S)Ph2 was added dropwise to soln. of Mn-complex under addition of triethylamine, 20 min; filtrated, concd., washed (hexane) (isolation of (CO)4MnSP(Ph)2C(O)N(Ph)), dimeric complex was isolated from hexane-filtrate (evapd.), both complexes chromd.; elem. anal.;