Technology Process of N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin
There total 6 articles about N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) HNO3, <2H2>sulfuric acid, 2.) sodium dichromate, H2SO4 / 1.) D2O, 1.5 h, 2.) H2O, reflux, 5 h
2: 2.43 g / PCl5 / 0.25 h / 60 °C
3: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature
4: 0.862 g / H2 / 10percent Pd/C / ethanol / 1 h
5: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr
With
sodium dichromate; phosphorus pentachloride; sulfuric acid; hydrogen; nitric acid; sulfuric acid-d2; triethylamine;
palladium on activated charcoal;
In
ethanol; benzene;
DOI:10.1002/jlcr.2580361010
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2.43 g / PCl5 / 0.25 h / 60 °C
2: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature
3: 0.862 g / H2 / 10percent Pd/C / ethanol / 1 h
4: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr
With
phosphorus pentachloride; hydrogen; triethylamine;
palladium on activated charcoal;
In
ethanol; benzene;
DOI:10.1002/jlcr.2580361010
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature
2: 0.862 g / H2 / 10percent Pd/C / ethanol / 1 h
3: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr
With
hydrogen; triethylamine;
palladium on activated charcoal;
In
ethanol; benzene;
DOI:10.1002/jlcr.2580361010
