N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

Base Information

Chemical Name:N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin
CAS No.:171777-70-1
Molecular Formula:C₂₅H₂₇N₇O₇
Molecular Weight:541.5
Hs Code.:

N(2')-acetyl-6-<N-(4-amino<2,3,5,6-2H4>benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

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Chemical Property of N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

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Technology Process of N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

There total 6 articles about N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2037-26-5
⁽²⁾H₈-toluene

: 171777-70-1
N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) HNO₃, <2H₂>sulfuric acid, 2.) sodium dichromate, H₂SO₄ / 1.) D₂O, 1.5 h, 2.) H₂O, reflux, 5 h

2: 2.43 g / PCl₅ / 0.25 h / 60 °C

3: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature

4: 0.862 g / H₂ / 10percent Pd/C / ethanol / 1 h

5: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr

With sodium dichromate; phosphorus pentachloride; sulfuric acid; hydrogen; nitric acid; sulfuric acid-d2; triethylamine; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/jlcr.2580361010

Reference yield:

: 171777-66-5
4-nitro<2,3,5,6-2H4>benzoic acid

: 171777-70-1
N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

Guidance literature:: Multi-step reaction with 4 steps

1: 2.43 g / PCl₅ / 0.25 h / 60 °C

2: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature

3: 0.862 g / H₂ / 10percent Pd/C / ethanol / 1 h

4: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr

With phosphorus pentachloride; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/jlcr.2580361010

Reference yield:

: 171777-67-6
4-nitro<2,3,5,6-2H4>benzoyl chloride

: 171777-70-1
N(2')-acetyl-6-benzoyl)-L-glutamic acid diethyl ester-azomethin>-pterin

Guidance literature:: Multi-step reaction with 3 steps

1: 2.39 g / triethylamine / benzene / 0.25 h / Ambient temperature

2: 0.862 g / H₂ / 10percent Pd/C / ethanol / 1 h

3: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/jlcr.2580361010