1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate

Base Information

• Chemical Name: 1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate
• CAS No.: 6992-72-9
• Molecular Formula: 2C₆H₁₅N₃O₃*3H₂O₄S
• Molecular Weight: 648.645
• Mol file: 6992-72-9.mol

Synonyms:

Chemical Property of 1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate

There total 3 articles about 1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

trinitrophloroglucinol (4328-17-0) → 1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate (6992-72-9,104973-97-9,110181-21-0)

Guidance literature:

With platinum(IV) oxide; sulfuric acid; hydrogen; In sulfuric acid; water; for 240h; under 6750.5 Torr;

DOI:10.1002/hlca.19900730110

Reference yield:

1,3,5-triacetoxybenzene (2999-40-8) → 1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate (6992-72-9,104973-97-9,110181-21-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) fuming, 100percent HNO₃, 50percent KOH, 2.) BaCl₂, 3.) 1m aq. H₂SO₄

2: 50 percent / H₂/PtO₂, aq. H₂SO₄ / H₂SO₄; H₂O / 240 h / 6750.5 Torr

With platinum(IV) oxide; potassium hydroxide; sulfuric acid; hydrogen; nitric acid; barium(II) chloride; In sulfuric acid; water;

DOI:10.1002/hlca.19900730110

Reference yield:

2,4,6-triamino-phloroglucinol; sulfate (117122-04-0) → 1,3,5-Triamino-1,3,5-trideoxy-cis-inositol sulfate (6992-72-9,104973-97-9,110181-21-0)

Guidance literature:

With water; platinum; Hydrogenation;

upstream raw materials:

2,4,6-triamino-phloroglucinol; sulfate

trinitrophloroglucinol

1,3,5-triacetoxybenzene