benzyl methyl(phenyl)phosphinate

Base Information

• Chemical Name: benzyl methyl(phenyl)phosphinate
• CAS No.: 4126-92-5
• Molecular Formula: C₁₄H₁₅O₂P
• Molecular Weight: 246.246
• Mol file: 4126-92-5.mol

Synonyms:

Chemical Property of benzyl methyl(phenyl)phosphinate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of benzyl methyl(phenyl)phosphinate

There total 2 articles about benzyl methyl(phenyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

methyl(phenyl)phosphineoxide (19315-13-0,102222-19-5,102222-20-8,891848-03-6) + benzaldehyde (100-52-7) → benzyl methyl(phenyl)phosphinate (4126-92-5)

Guidance literature:

With caesium carbonate; In ethyl acetate; at 80 ℃; for 10h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.orglett.0c01537

Reference yield:

methyl methylphenylphosphinate (6389-79-3) → benzyl methyl(phenyl)phosphinate (4126-92-5)

Guidance literature:

Multi-step reaction with 2 steps

1: COCl₂ / CCl₄

2: Et₃N / diethyl ether

With triethylamine; In tetrachloromethane; diethyl ether;

DOI:10.1039/jr9630001004

upstream raw materials:

methyl methylphenylphosphinate

methyl(phenyl)phosphineoxide

benzaldehyde