(R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate

Base Information

Chemical Name:(R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate
CAS No.:1432740-77-6
Molecular Formula:C₂₁H₂₂ClN₃O₂
Molecular Weight:383.878
Hs Code.:

Synonyms:

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Chemical Property of (R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate

Chemical Property:

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Technology Process of (R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate

There total 3 articles about (R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24155-45-1
(R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethanol

: 31027-31-3
4-isopropylphenylisocyanate

: 1432740-77-6
(R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate

Guidance literature:: (R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethanol; With sodium hydride; In acetonitrile; at 20 ℃; for 2h;

4-isopropylphenylisocyanate; at 20 ℃; for 24h;
DOI:10.1021/jm500739f

Reference yield:

: 536-38-9
4-chlorobenzoylmethyl bromide

: 1432740-77-6
(R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 2 h / 0 °C

2.1: Noyori's catalyst; formic acid; triethylamine / dichloromethane / 26 h / 40 °C / Inert atmosphere

3.1: sodium hydride / acetonitrile / 2 h / 20 °C

3.2: 24 h / 20 °C

With Noyori's catalyst; formic acid; sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm500739f

Reference yield:

: 24155-32-6
1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-one

: 1432740-77-6
(R)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl 4-isopropylphenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Noyori's catalyst; formic acid; triethylamine / dichloromethane / 26 h / 40 °C / Inert atmosphere

2.1: sodium hydride / acetonitrile / 2 h / 20 °C

2.2: 24 h / 20 °C

With Noyori's catalyst; formic acid; sodium hydride; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jm500739f