(7-Methoxy-1-benzofuran-2-yl)methanol

Base Information

• Chemical Name: (7-Methoxy-1-benzofuran-2-yl)methanol
• CAS No.: 75566-54-0
• Molecular Formula: C₁₀H₁₀O₃
• Molecular Weight: 178.188
• DSSTox Substance ID: DTXSID70472639
• Nikkaji Number: J2.652.052E
• Wikidata: Q82301656

Synonyms:75566-54-0;(7-methoxy-1-benzofuran-2-yl)methanol;2-(Hydroxymethyl)-7-methoxybenzofuran;(7-methoxybenzofuran-2-yl)methanol;2-Benzofuranmethanol, 7-methoxy-;SCHEMBL73352;7-methoxybenzofuran-2-ylmethanol;DTXSID70472639;7-methoxy-benzofuran-2-ylmethanol;VXDZMYNEZZENIT-UHFFFAOYSA-N;7-Methoxybenzofuran-2-yl-methanol;2-hydroxymethyl-7-methoxybenzofuran;AC6761;MFCD12047731;AKOS005208281;SY045638;CS-0303259;EN300-239023;A915150;F2147-0218

Chemical Property of (7-Methoxy-1-benzofuran-2-yl)methanol

Chemical Property:

• XLogP3: 1.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 178.062994177
• Heavy Atom Count: 13
• Complexity: 172

Purity/Quality:

97% ^*data from raw suppliers

2-(Hydroxymethyl)-7-methoxybenzofuran 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC2=C1OC(=C2)CO

Technology Process of (7-Methoxy-1-benzofuran-2-yl)methanol

There total 6 articles about (7-Methoxy-1-benzofuran-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

7-methoxybenzofuran-2-carboxylic acid (4790-79-8) → 2-hydroxymethyl-7-methoxy-benzofuran (75566-54-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0041-1737275

Reference yield: 95.0%

7-Methoxybenzofuran-2-carbaldehyde (88234-77-9) → 2-hydroxymethyl-7-methoxy-benzofuran (75566-54-0)

Guidance literature:

With sodium tetrahydroborate; In ethanol; chloroform;

DOI:10.1007/s11172-007-0053-9

Reference yield: 86.0%

7-methoxy-2-methylene-2,3-dihydro-1-benzofuran-3-ol (1060729-00-1) → 2-hydroxymethyl-7-methoxy-benzofuran (75566-54-0)

Guidance literature:

With sulfuric acid; water; In 1,2-dimethoxyethane; at 40 ℃; for 15h; Inert atmosphere;

DOI:10.1021/jo801444n

upstream raw materials:

7-methoxybenzofuran-2-carboxylic acid

7-Methoxybenzofuran-2-carbaldehyde

3-methoxy-2-hydroxybenzaldehyde

2-carbomethoxy-7-methoxybenzofuran

Downstream raw materials:

7-Methoxybenzofuran-2-carbaldehyde

7-Hydroxy-2-hydroxymethyl-benzofuran

7-methoxy-2-methylbenzo[b]furan

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