C₂₂H₂₁N₃O₄*ClH

Base Information

Chemical Name:C₂₂H₂₁N₃O₄*ClH
CAS No.:911289-32-2
Molecular Formula:C₂₂H₂₁N₃O₄*ClH
Molecular Weight:427.887
Hs Code.:

C<sub>22</sub>H<sub>21</sub>N<sub>3</sub>O<sub>4</sub>*ClH

Synonyms:

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Chemical Property of C₂₂H₂₁N₃O₄*ClH

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Technology Process of C₂₂H₂₁N₃O₄*ClH

There total 13 articles about C₂₂H₂₁N₃O₄*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 911289-61-7
C₃₆H₃₃N₃O₄

: 911289-32-2,1273028-31-1
C₂₂H₂₁N₃O₄*ClH

Guidance literature:: With boron trichloride; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.bmc.2010.12.007

Reference yield:

: 118-71-8
Maltol

: 911289-32-2,1273028-31-1
C₂₂H₂₁N₃O₄*ClH

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydroxide / methanol; water / Reflux

1.2: 6 h / Reflux

2.1: ammonia / ethanol / Reflux

3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 °C / Reflux

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

5.1: 1 h / 130 °C

6.1: sodium hydroxide / ethanol / 2 h / Reflux

7.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / chloroform / 20 °C / Cooling with ice

8.1: sodium chlorite; aminosulfonic acid / water; acetone / 3 h / 20 °C

9.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

9.2: 12 h / 20 °C

10.1: boron trichloride / dichloromethane / 3 h / 0 °C

With sodium chlorite; aminosulfonic acid; ammonia; sulfur trioxide pyridine complex; boron trichloride; benzotriazol-1-ol; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; acetone;
DOI:10.1016/j.bmc.2010.12.007

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 911289-32-2,1273028-31-1
C₂₂H₂₁N₃O₄*ClH

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C / 760.05 Torr

3.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

3.2: 12 h / 20 °C

4.1: boron trichloride / dichloromethane / 3 h / 0 °C

With dmap; palladium 10% on activated carbon; hydrogen; boron trichloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2010.12.007