C₂₀H₂₆⁽²⁾H₂N₂O₂

Base Information

Chemical Name:C₂₀H₂₆⁽²⁾H₂N₂O₂
CAS No.:1448750-41-1
Molecular Formula:C₂₀H₂₈N₂O₂
Molecular Weight:330.439
Hs Code.:

C<sub>20</sub>H<sub>26</sub><sup>(2)</sup>H<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₆⁽²⁾H₂N₂O₂

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Technology Process of C₂₀H₂₆⁽²⁾H₂N₂O₂

There total 2 articles about C₂₀H₂₆⁽²⁾H₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1448750-46-6
C₁₉H₂₆⁽²⁾H₃N₂⁽¹⁺⁾*I^(1-)

: 1448750-41-1
C₂₀H₂₆⁽²⁾H₂N₂O₂

: C₂₀H₂₄⁽²⁾H₄N₂O₂

Guidance literature:: C₁₉H₂₆⁽²⁾H₃N₂⁽¹⁺⁾*I^(1-); With potassium hydride; In tetrahydrofuran; at 20 ℃; for 48h; Darkness; Schlenk technique; Inert atmosphere;

carbon dioxide; In tetrahydrofuran; at -78 - 20 ℃; for 2h; under 760.051 Torr; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja405114e

Reference yield:

: 25364-47-0
1-(2,6-diisopropylphenyl)-1H-imidazole

: 1448750-41-1
C₂₀H₂₆⁽²⁾H₂N₂O₂

: C₂₀H₂₄⁽²⁾H₄N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 - -20 °C / Schlenk technique; Inert atmosphere

1.2: 0.17 h / -78 - 0 °C / Schlenk technique; Inert atmosphere

2.1: acetonitrile / 24 h / 80 °C / Schlenk technique; Inert atmosphere

3.1: potassium hydride / tetrahydrofuran / 48 h / 20 °C / Darkness; Schlenk technique; Inert atmosphere

3.2: 2 h / -78 - 20 °C / 760.05 Torr / Schlenk technique; Inert atmosphere

With n-butyllithium; potassium hydride; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1021/ja405114e