cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II)

Base Information

Chemical Name:cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II)
CAS No.:102920-75-2
Molecular Formula:C₅₂H₇₀N₄O₂P₄PtS₂
Molecular Weight:1166.26
Hs Code.:

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Chemical Property of cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II)

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Technology Process of cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II)

There total 2 articles about cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 29894-57-3
dioxygenbis(triphenylphosphine)platinum⁽⁰⁾

: 102870-32-6
bis(tert-butylamido)thiophosphoric acid O-trimethylsilylester

: 102920-75-2
cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II)

Guidance literature:: In acetonitrile; byproducts: P(C6H5)3, bis(trimethylsilyl)peroxide; Ar, silylester added to a suspension of Pt-compound in CH3CN at room temp., stirred until the solution is clear; solvent removed in vacuo, washed (pentane, -20°C), dried for 4 h at 0.01 Torr;

Reference yield: 73.0%

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 102870-33-7
Natrium-bis(tert-butylamido)thiophosphat

: 102920-75-2
cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II)

Guidance literature:: In acetonitrile; byproducts: NaCl; Ar, Pt-complex added at room temp. to a suspension of Na(C(CH3)3NH)2P(S)O, stirred for 2 h; centrifugated, solution separated from NaCl, NaCl washed with acetonitrile, zentrifugate and wash solution combined, solvent removed in vacuo, washed (pentane), dried for 2 h at 0.01 Torr; elem. anal.;

Reference yield: 76.0%

: 102920-75-2
cis-bis[N,N'-di(tert-butyl)diamidothiophosphato-S]bis(triphenylphosphane)platinum(II)

: 102920-76-3
trans-[N,N'-di(tert-butyl)diamidothiophosphato-S][N,N'-di(tert-butyl)diamidothiophosphato-N,S](triphenylphosphane)platinum(II)

Guidance literature:: With S₈; In toluene; byproducts: (C6H5)3PS; Ar, S8 added at room temp. to Pt-complex in toluene, stirred for 24 h; solvent removed in vacuo, ppt. dissolved in a mimimum amt. of CH2Cl2; chromy. (silicagel, ether), solvent removed, washed (pentane), dried for 4 h at 0.01 Torr; elem. anal.;