[Pt(1,2-bis(diphenylphosphino)ethane)(1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]BF₄

Base Information

• Chemical Name: [Pt(1,2-bis(diphenylphosphino)ethane)(1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]BF₄
• CAS No.: 1188508-77-1
• Molecular Formula: BF₄*C₆₀H₅₆O₃P₃Pt
• Molecular Weight: 1199.91

Synonyms:

Chemical Property of [Pt(1,2-bis(diphenylphosphino)ethane)(1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]BF₄

Chemical Property:

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Technology Process of [Pt(1,2-bis(diphenylphosphino)ethane)(1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]BF₄

There total 1 articles about [Pt(1,2-bis(diphenylphosphino)ethane)(1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

silver tetrafluoroborate (14104-20-2) + [Pt(μ-Cl)(κ2-(R)-1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]2 (1188508-70-4,1188553-34-5) + 1,2-bis-(diphenylphosphino)ethane (1663-45-2) → [Pt(1,2-bis(diphenylphosphino)ethane)(1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]BF4 (1188508-77-1)

Guidance literature:

In dichloromethane; byproducts: AgCl; (N2); using Schlenk techniques; dissolving of (PtCl((t-Bu)2C6H2OP(OC10H6)2))2, AgBF4 and dppe (2 equiv.) in CH2Cl2; stirring at room temp. for 1h; filtration, washing of filter cake with CH2Cl2; concn. of combined filtrate on rotavapor; pptn. by addn. of hexanes; centrifuging; quickly washing with cold hexanes; thorough drying under vac., elem. anal.;

DOI:10.1021/om9003237

upstream raw materials:

silver tetrafluoroborate

[Pt(μ-Cl)(κ2-(R)-1,1'-binaphthane-2,2'-diyl 2,4-di-tert-butylphenyl phosphite(-1H))]2

1,2-bis-(diphenylphosphino)ethane

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