NiCl₃(cis-bis(diphenylphosphino)ethylene)

Base Information

Chemical Name:NiCl₃(cis-bis(diphenylphosphino)ethylene)
CAS No.:90526-44-6
Molecular Formula:C₂₆H₂₂Cl₃NiP₂
Molecular Weight:561.457
Hs Code.:

NiCl<SUB>3</SUB>(cis-bis(diphenylphosphino)ethylene)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of NiCl₃(cis-bis(diphenylphosphino)ethylene)

Chemical Property:

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Technology Process of NiCl₃(cis-bis(diphenylphosphino)ethylene)

There total 3 articles about NiCl₃(cis-bis(diphenylphosphino)ethylene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52564-34-8,23443-96-1,42584-04-3
NiCl2(cis-1,2-bis(diphenylphosphino)ethene)

: 90526-44-6
NiCl₃(cis-bis(diphenylphosphino)ethylene)

Guidance literature:: With chlorine; In tetrachloromethane; suspn. (Ni((C6H5)2PCHCHP(C6H5)2)Cl2) in dry CCl4 treated with Br2 in CCl4 and stirred for 30 min; complex filtered off, rinsed with dry CCl4 and dried in vacuo; elem. anal.;

Reference yield:

: 52564-34-8,23443-96-1,42584-04-3
(Ph₂PCH=CHPPh₂)NiCl₂

: 932-72-9
(Dichloroiodo)benzene

: 90526-44-6
NiCl₃(cis-bis(diphenylphosphino)ethylene)

Guidance literature:: In acetonitrile; at 23 ℃; for 0.0833333h; Inert atmosphere; Glovebox; Darkness;
DOI:10.1021/acs.organomet.5b00568

Reference yield:

: 52564-34-8,23443-96-1,42584-04-3
NiCl2(cis-1,2-bis(diphenylphosphino)ethene)

: 2696-92-6
nitrosylchloride

: 90526-44-6
NiCl₃(cis-bis(diphenylphosphino)ethylene)

Guidance literature:: In dichloromethane; excess NOCl slowly carried in stream dry N2 through 0°C trap containing stirred soln. (Ni(Ph2PCHCHPPh2)Cl2) in CH2Cl2; solvent pumped off, solid filtered off and dried; elem. anal.;