diiodobis(2-(m-tolylazo)pyridine)ruthenium(II)

Base Information

Chemical Name:diiodobis(2-(m-tolylazo)pyridine)ruthenium(II)
CAS No.:77321-11-0
Molecular Formula:C₂₄H₂₂I₂N₆Ru
Molecular Weight:749.358
Hs Code.:

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Chemical Property of diiodobis(2-(m-tolylazo)pyridine)ruthenium(II)

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Technology Process of diiodobis(2-(m-tolylazo)pyridine)ruthenium(II)

There total 1 articles about diiodobis(2-(m-tolylazo)pyridine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 87014-42-4
2-(3-methylphenylazo)pyridine

: 14898-67-0
ruthenium(III) chloride trihydrate

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 77321-11-0
diiodobis(2-(m-tolylazo)pyridine)ruthenium(II)

Guidance literature:: In methanol; N2 was passed for 15 min through soln. of RuCl3*3H2O in MeOH, NaI was added, mixt. was stirred for 45 min at room temp., soln. of ligand in MeOH was added, mixt. was stirred for 8 h; filtered, washed with H2O and Et2O, dried in vac. desiccator over P4O10, ppt. was dissolved in CHCl3, chromy. on silica gel column, eluted withC6H6, evapd. at room temp.; elem. anal.;
DOI:10.1021/ic50221a061