IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2

Base Information

Chemical Name:IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2
CAS No.:90634-55-2
Molecular Formula:C₄₈H₃₆ClF₄IrSb₂
Molecular Weight:1159.98
Hs Code.:

IrCl(C<sub>6</sub>F<sub>4</sub>C<sub>6</sub>H<sub>6</sub>)(Sb(C<sub>6</sub>H<sub>5</sub>)3)2

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Chemical Property of IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2

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Technology Process of IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2

There total 1 articles about IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 88478-63-1
{IrCl(tetrafluorobenzobarrelene)2}

: 603-36-1
triphenylantimony

: 90634-55-2
IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2

Guidance literature:: In acetone; complex suspn. treated with ligand for 15 min; concd. (vac.), pptd. (hexane), filtered off, washed (hexane), dried (vac.); elem. anal.;
DOI:10.1016/0022-328X(84)85014-7

Reference yield: 65.0%

: 90634-55-2
IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2

: silver perchlorate

: 90634-84-7
[Ir(C₆F₄C₆H₆)(Sb(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Ir(C₆F₄C₆H₆)(Sb(C₆H₅)3)2]ClO₄

Guidance literature:: In dichloromethane; acetone; byproducts: AgCl; under N2 and protected from daylight complex in CH2Cl2 treated for 30 min with AgClO4 in acetone; AgCl filtered off, filtrate concd. (vac.), pptd. (ether), filtered off,washed with ether, dried in vac.; elem. anal.;
DOI:10.1016/0022-328X(84)85014-7

Reference yield: 50.0%

: 10025-69-1
tin(II) chloride dihdyrate

: 90634-55-2
IrCl(C₆F₄C₆H₆)(Sb(C₆H₅)3)2

: Ir(SnCl₃)(C₆F₄C₆H₆)(Sb(C₆H₅)3)2

Guidance literature:: In acetone; complex soln. treated with SnCl2*2H2O for 10 min; concd. (vac.), pptd. (hexane), filtered off, washed with hexane, dried (vac.); elem. anal.;
DOI:10.1016/0022-328X(84)85014-7