Dihydro-5-(4-methoxyphenyl)-2,2-dimethyl-3(2H)-furanone oxime

Base Information

Chemical Name:Dihydro-5-(4-methoxyphenyl)-2,2-dimethyl-3(2H)-furanone oxime
CAS No.:327982-94-5
Molecular Formula:C₁₃H₁₇NO₃
Molecular Weight:235.283
Hs Code.:
DSSTox Substance ID:DTXSID301182561

Synonyms:Oprea1_492656;DTXSID301182561;HMS2407P24;Dihydro-5-(4-methoxyphenyl)-2,2-dimethyl-3(2H)-furanone oxime;327982-94-5

Suppliers and Price of Dihydro-5-(4-methoxyphenyl)-2,2-dimethyl-3(2H)-furanone oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dihydro-5-(4-methoxyphenyl)-2,2-dimethyl-3(2H)-furanone oxime

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:235.12084340
Heavy Atom Count:17
Complexity:293

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(C(=NO)CC(O1)C2=CC=C(C=C2)OC)C

Technology Process of Dihydro-5-(4-methoxyphenyl)-2,2-dimethyl-3(2H)-furanone oxime

There total 4 articles about Dihydro-5-(4-methoxyphenyl)-2,2-dimethyl-3(2H)-furanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 81791-31-3
5-(4-methoxy-phenyl)-2,2-dimethyl-dihydro-furan-3-one

: 327982-94-5
5-(4-methoxyphenyl)-2,2-dimethyltetrahydrofuran-3-one oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; for 5h; regioselective reaction; Reflux;
DOI:10.1007/s11172-012-0088-4

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 327982-94-5
5-(4-methoxyphenyl)-2,2-dimethyltetrahydrofuran-3-one oxime

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; water / 45 - 50 °C

2: phosphoric acid / 100 °C

3: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 5 h / Reflux

With phosphoric acid; hydroxylamine hydrochloride; sodium acetate; potassium hydroxide; In ethanol; water;
DOI:10.1007/s11172-012-0088-4

Reference yield:

: 98017-82-4
C₁₃H₁₆O₃

: 327982-94-5
5-(4-methoxyphenyl)-2,2-dimethyltetrahydrofuran-3-one oxime

Guidance literature:: Multi-step reaction with 2 steps

1: phosphoric acid / 100 °C

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 5 h / Reflux

With phosphoric acid; hydroxylamine hydrochloride; sodium acetate; In ethanol; water;
DOI:10.1007/s11172-012-0088-4