2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester

Base Information

• Chemical Name: 2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester
• CAS No.: 10235-84-4
• Molecular Formula: C₁₉H₁₆O₄
• Molecular Weight: 308.334
• Mol file: 10235-84-4.mol

Synonyms:

Chemical Property of 2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester

There total 1 articles about 2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 2-phenyl-indene-5,6-dicarboxylic acid anhydride (10235-79-7) → 2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester (10235-84-4)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/jo01277a011

Reference yield:

2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester (10235-84-4) → 2-Phenyl-indan-5,6-dicarbonsaeure-dimethylester

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1021/jo01277a011

Reference yield:

2-Phenyl-inden-5,6-dicarbonsaeure-dimethylester (10235-84-4) → 5,6-Bis-brommethyl-2-phenyl-indan (10231-95-5)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd-C

2: LiAlH₄

3: Py, PBr₃

With pyridine; lithium aluminium tetrahydride; hydrogen; phosphorus tribromide; palladium on activated charcoal;

DOI:10.1021/jo01277a011

upstream raw materials:

methanol

2-phenyl-indene-5,6-dicarboxylic acid anhydride

Downstream raw materials:

5,6-Bis-brommethyl-2-phenyl-inden

5,6-Bis-brommethyl-2-phenyl-indan

6,8-Dimethyl-2,7-diphenyl-1,7-dihydro-cycloheptinden-7-ol

5,6-Bis-hydroxy-methyl-2-phenyl-indan