N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid

Base Information

Chemical Name:N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid
CAS No.:50557-87-4
Molecular Formula:C₁₆H₂₃N₃O₄
Molecular Weight:321.376
Hs Code.:

N<sup>α</sup>-Acetyl-N<sup>ε</sup>-benzyloxycarbonyl-L-lysinamid

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid

Chemical Property:

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Technology Process of N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid

There total 5 articles about N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27894-50-4
methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride

: 108-24-7
acetic anhydride

: 50557-87-4
N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid

Guidance literature:: methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride; acetic anhydride; With sodium hydroxide; In water; at -0.16 ℃; for 2h;

With ammonia; In methanol; at 20 ℃; Further stages.;
DOI:10.1016/j.jct.2006.03.015

Reference yield:

: 55592-81-9
N^ε-(benzyloxycarbonyl)-N^α-(tert-butoxycarbonyl)-L-lysinamide

: 50557-87-4
N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / formic acid

2: Py, N-ethylmorpholine / dimethylformamide

With N-ethylmorpholine;; pyridine; hydrogenchloride; In formic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19750580724

Reference yield:

: 2389-46-0
N-α-tert-butyloxycarbonyl-N-ε-benzyloxycarbonyl-lysine p-nitrophenyl ester

: 50557-87-4
N^α-Acetyl-N^ε-benzyloxycarbonyl-L-lysinamid

Guidance literature:: Multi-step reaction with 3 steps

1: NH₃ / acetonitrile

2: aq. HCl / formic acid

3: Py, N-ethylmorpholine / dimethylformamide

With N-ethylmorpholine;; pyridine; hydrogenchloride; ammonia; In formic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/hlca.19750580724