Benzaldehyde, 2-[(acetyloxy)methyl]-3-methoxy-

Base Information

Chemical Name:Benzaldehyde, 2-[(acetyloxy)methyl]-3-methoxy-
CAS No.:130662-46-3
Molecular Formula:C11H12O4
Molecular Weight:208.214
Hs Code.:
DSSTox Substance ID:DTXSID70464372
Nikkaji Number:J1.832.740F
Wikidata:Q82289662

Synonyms:130662-46-3;Benzaldehyde, 2-[(acetyloxy)methyl]-3-methoxy-;DTXSID70464372

Suppliers and Price of Benzaldehyde, 2-[(acetyloxy)methyl]-3-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzaldehyde, 2-[(acetyloxy)methyl]-3-methoxy-

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:208.07355886
Heavy Atom Count:15
Complexity:227

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OCC1=C(C=CC=C1OC)C=O

Technology Process of Benzaldehyde, 2-[(acetyloxy)methyl]-3-methoxy-

There total 4 articles about Benzaldehyde, 2-[(acetyloxy)methyl]-3-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 71785-97-2
2-(bromomethyl)-3-(dibromomethyl)anisole

: 130662-46-3
2-(acetyloxymethyl)-3-methoxybenzaldehyde

Guidance literature:: With sodium acetate; acetic acid; for 3h; Heating;

Reference yield: 88.0%

: 127-09-3
sodium acetate

: 71785-97-2
2-(bromomethyl)-3-(dibromomethyl)anisole

: 130662-46-3
2-(acetyloxymethyl)-3-methoxybenzaldehyde

Guidance literature:: sodium acetate; 2-(bromomethyl)-3-(dibromomethyl)anisole; In acetic acid; for 29h; Reflux;

With hydrogenchloride; In water; acetic acid; at 25 ℃; for 2h;
DOI:10.1002/ejoc.200801070

Reference yield:

: 526-75-0
2,3-Dimethylphenol

: 130662-46-3
2-(acetyloxymethyl)-3-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / tetra-N-butylammonium hydrogensulfate, aq. potassium hydroxide / CH₂Cl₂ / 2 h / Ambient temperature

2: 98 percent / N-bromosuccinimide (NBS) / CCl₄ / 3 h / Heating; Irradiation

3: 97 percent / sodium acetate, glacial acetic acid / 3 h / Heating

With potassium hydroxide; N-Bromosuccinimide; sodium acetate; tetra(n-butyl)ammonium hydrogensulfate; acetic acid; In tetrachloromethane; dichloromethane;